| Ni1—Cl2 | 2.4762 (11) | C2—H2B | 0.9500 |
| Ni1—Cl3 | 2.3964 (10) | C25—H25A | 0.9900 |
| Ni1—Cl1 | 2.4408 (12) | C25—H25B | 0.9900 |
| Ni1—N1 | 2.077 (3) | C25—C24 | 1.495 (6) |
| Ni1—N3 | 2.041 (3) | C25—C26 | 1.536 (8) |
| Ni1—N2 | 2.126 (4) | C7—C13 | 1.545 (5) |
| Ni2—Cl2 | 2.4216 (10) | C4—H4 | 0.9500 |
| Ni2—Cl3 | 2.4128 (12) | C24—C23 | 1.516 (7) |
| Ni2—Cl4 | 2.4077 (14) | C6—H6A | 0.9900 |
| Ni2—N6 | 2.027 (3) | C6—H6B | 0.9900 |
| Ni2—N5 | 2.103 (4) | C10—H10 | 1.0000 |
| Ni2—N4 | 2.095 (4) | C10—C11 | 1.540 (8) |
| O1—H1 | 0.85 (7) | C23—C28 | 1.550 (8) |
| O1—N3 | 1.403 (5) | C23—C29 | 1.502 (9) |
| N1—C5 | 1.345 (6) | C15—H15A | 0.9500 |
| N1—C1 | 1.338 (5) | C15—H15B | 0.9500 |
| N3—C8 | 1.269 (6) | C31—H31A | 0.9500 |
| N2—H2 | 0.77 (5) | C31—H31B | 0.9500 |
| N2—C7 | 1.503 (5) | C13—H13A | 0.9800 |
| N2—C6 | 1.477 (5) | C13—H13B | 0.9800 |
| O2—H2A | 0.76 (8) | C13—H13C | 0.9800 |
| O2—N6 | 1.385 (5) | C11—H11A | 0.9900 |
| C8—C9 | 1.509 (6) | C11—H11B | 0.9900 |
| C8—C7 | 1.513 (7) | C16—H16A | 0.9800 |
| C5—C4 | 1.385 (6) | C16—H16B | 0.9800 |
| C5—C6 | 1.508 (6) | C16—H16C | 0.9800 |
| N6—C24 | 1.269 (6) | C18—H18 | 0.9500 |
| N5—H5 | 0.93 (7) | C18—C17 | 1.370 (8) |
| N5—C23 | 1.517 (7) | C18—C19 | 1.318 (12) |
| N5—C22 | 1.524 (9) | C17—H17 | 0.9500 |
| C12—H12A | 0.9900 | C26—H26 | 1.0000 |
| C12—H12B | 0.9900 | C26—C27 | 1.532 (10) |
| C12—C7 | 1.555 (6) | C21—C22 | 1.457 (12) |
| C12—C11 | 1.528 (7) | C21—C20 | 1.465 (10) |
| C14—C10 | 1.523 (6) | C28—H28A | 0.9900 |
| C14—C15 | 1.326 (7) | C28—H28B | 0.9900 |
| C14—C16 | 1.506 (7) | C28—C27 | 1.525 (9) |
| C3—H3 | 0.9500 | C32—H32A | 0.9800 |
| C3—C2 | 1.373 (8) | C32—H32B | 0.9800 |
| C3—C4 | 1.384 (7) | C32—H32C | 0.9800 |
| C9—H9A | 0.9900 | C22—H22A | 0.9900 |
| C9—H9B | 0.9900 | C22—H22B | 0.9900 |
| C9—C10 | 1.545 (7) | C27—H27A | 0.9900 |
| C1—H1A | 0.9500 | C27—H27B | 0.9900 |
| C1—C2 | 1.396 (6) | C29—H29A | 0.9800 |
| C30—C31 | 1.318 (8) | C29—H29B | 0.9800 |
| C30—C26 | 1.521 (8) | C29—H29C | 0.9800 |
| C30—C32 | 1.503 (8) | C19—H19 | 0.9500 |
| N4—C17 | 1.359 (8) | C19—C20 | 1.360 (13) |
| N4—C21 | 1.314 (8) | C20—H20 | 0.9500 |
| Cl3—Ni1—Cl2 | 84.13 (4) | C8—C7—C13 | 108.0 (4) |
| Cl3—Ni1—Cl1 | 91.99 (4) | C13—C7—C12 | 110.9 (4) |
| Cl1—Ni1—Cl2 | 100.61 (4) | C5—C4—H4 | 120.7 |
| N1—Ni1—Cl2 | 88.69 (10) | C3—C4—C5 | 118.5 (5) |
| N1—Ni1—Cl3 | 171.31 (10) | C3—C4—H4 | 120.7 |
| N1—Ni1—Cl1 | 94.14 (11) | N6—C24—C25 | 124.3 (5) |
| N1—Ni1—N2 | 79.91 (13) | N6—C24—C23 | 116.7 (4) |
| N3—Ni1—Cl2 | 170.10 (12) | C25—C24—C23 | 118.8 (4) |
| N3—Ni1—Cl3 | 94.30 (9) | N2—C6—C5 | 110.5 (4) |
| N3—Ni1—Cl1 | 89.21 (12) | N2—C6—H6A | 109.6 |
| N3—Ni1—N1 | 91.94 (13) | N2—C6—H6B | 109.6 |
| N3—Ni1—N2 | 77.38 (15) | C5—C6—H6A | 109.6 |
| N2—Ni1—Cl2 | 93.02 (10) | C5—C6—H6B | 109.6 |
| N2—Ni1—Cl3 | 95.56 (9) | H6A—C6—H6B | 108.1 |
| N2—Ni1—Cl1 | 165.04 (11) | C14—C10—C9 | 114.7 (4) |
| Cl3—Ni2—Cl2 | 84.97 (4) | C14—C10—H10 | 106.7 |
| Cl4—Ni2—Cl2 | 99.38 (4) | C14—C10—C11 | 111.4 (4) |
| Cl4—Ni2—Cl3 | 93.14 (5) | C9—C10—H10 | 106.7 |
| N6—Ni2—Cl2 | 171.72 (12) | C11—C10—C9 | 110.3 (4) |
| N6—Ni2—Cl3 | 92.13 (11) | C11—C10—H10 | 106.7 |
| N6—Ni2—Cl4 | 88.51 (11) | N5—C23—C28 | 112.0 (5) |
| N6—Ni2—N5 | 79.29 (16) | C24—C23—N5 | 109.5 (4) |
| N6—Ni2—N4 | 88.11 (15) | C24—C23—C28 | 108.9 (4) |
| N5—Ni2—Cl2 | 93.15 (13) | C29—C23—N5 | 104.7 (5) |
| N5—Ni2—Cl3 | 94.06 (15) | C29—C23—C24 | 109.9 (5) |
| N5—Ni2—Cl4 | 166.04 (12) | C29—C23—C28 | 111.8 (5) |
| N4—Ni2—Cl2 | 93.92 (11) | C14—C15—H15A | 120.0 |
| N4—Ni2—Cl3 | 173.62 (15) | C14—C15—H15B | 120.0 |
| N4—Ni2—Cl4 | 93.24 (16) | H15A—C15—H15B | 120.0 |
| N4—Ni2—N5 | 79.7 (2) | C30—C31—H31A | 120.0 |
| Ni2—Cl2—Ni1 | 91.88 (4) | C30—C31—H31B | 120.0 |
| Ni1—Cl3—Ni2 | 94.09 (4) | H31A—C31—H31B | 120.0 |
| N3—O1—H1 | 111 (4) | C7—C13—H13A | 109.5 |
| C5—N1—Ni1 | 113.6 (3) | C7—C13—H13B | 109.5 |
| C1—N1—Ni1 | 127.6 (3) | C7—C13—H13C | 109.5 |
| C1—N1—C5 | 118.8 (4) | H13A—C13—H13B | 109.5 |
| O1—N3—Ni1 | 121.4 (3) | H13A—C13—H13C | 109.5 |
| C8—N3—Ni1 | 122.2 (3) | H13B—C13—H13C | 109.5 |
| C8—N3—O1 | 115.9 (3) | C12—C11—C10 | 112.0 (4) |
| Ni1—N2—H2 | 93 (4) | C12—C11—H11A | 109.2 |
| C7—N2—Ni1 | 113.6 (3) | C12—C11—H11B | 109.2 |
| C7—N2—H2 | 116 (4) | C10—C11—H11A | 109.2 |
| C6—N2—Ni1 | 104.0 (2) | C10—C11—H11B | 109.2 |
| C6—N2—H2 | 109 (4) | H11A—C11—H11B | 107.9 |
| C6—N2—C7 | 118.1 (3) | C14—C16—H16A | 109.5 |
| N6—O2—H2A | 105 (5) | C14—C16—H16B | 109.5 |
| N3—C8—C9 | 124.7 (4) | C14—C16—H16C | 109.5 |
| N3—C8—C7 | 116.1 (4) | H16A—C16—H16B | 109.5 |
| C9—C8—C7 | 119.2 (4) | H16A—C16—H16C | 109.5 |
| N1—C5—C4 | 122.3 (4) | H16B—C16—H16C | 109.5 |
| N1—C5—C6 | 115.1 (4) | C17—C18—H18 | 121.9 |
| C4—C5—C6 | 122.6 (4) | C19—C18—H18 | 121.9 |
| O2—N6—Ni2 | 122.4 (3) | C19—C18—C17 | 116.1 (8) |
| C24—N6—Ni2 | 120.3 (3) | N4—C17—C18 | 124.7 (7) |
| C24—N6—O2 | 116.7 (4) | N4—C17—H17 | 117.7 |
| Ni2—N5—H5 | 94 (4) | C18—C17—H17 | 117.7 |
| C23—N5—Ni2 | 112.0 (3) | C30—C26—C25 | 114.3 (5) |
| C23—N5—H5 | 115 (4) | C30—C26—H26 | 107.1 |
| C23—N5—C22 | 118.6 (4) | C30—C26—C27 | 112.5 (5) |
| C22—N5—Ni2 | 102.9 (4) | C25—C26—H26 | 107.1 |
| C22—N5—H5 | 110 (4) | C27—C26—C25 | 108.5 (5) |
| H12A—C12—H12B | 107.8 | C27—C26—H26 | 107.1 |
| C7—C12—H12A | 109.0 | N4—C21—C22 | 116.4 (5) |
| C7—C12—H12B | 109.0 | N4—C21—C20 | 117.2 (8) |
| C11—C12—H12A | 109.0 | C22—C21—C20 | 126.3 (7) |
| C11—C12—H12B | 109.0 | C23—C28—H28A | 109.2 |
| C11—C12—C7 | 113.0 (4) | C23—C28—H28B | 109.2 |
| C15—C14—C10 | 124.9 (4) | H28A—C28—H28B | 107.9 |
| C15—C14—C16 | 120.2 (4) | C27—C28—C23 | 112.2 (6) |
| C16—C14—C10 | 114.9 (4) | C27—C28—H28A | 109.2 |
| C2—C3—H3 | 120.1 | C27—C28—H28B | 109.2 |
| C2—C3—C4 | 119.7 (4) | C30—C32—H32A | 109.5 |
| C4—C3—H3 | 120.1 | C30—C32—H32B | 109.5 |
| C8—C9—H9A | 109.2 | C30—C32—H32C | 109.5 |
| C8—C9—H9B | 109.2 | H32A—C32—H32B | 109.5 |
| C8—C9—C10 | 112.2 (4) | H32A—C32—H32C | 109.5 |
| H9A—C9—H9B | 107.9 | H32B—C32—H32C | 109.5 |
| C10—C9—H9A | 109.2 | N5—C22—H22A | 109.7 |
| C10—C9—H9B | 109.2 | N5—C22—H22B | 109.7 |
| N1—C1—H1A | 119.0 | C21—C22—N5 | 110.0 (4) |
| N1—C1—C2 | 122.1 (4) | C21—C22—H22A | 109.7 |
| C2—C1—H1A | 119.0 | C21—C22—H22B | 109.7 |
| C31—C30—C26 | 124.8 (5) | H22A—C22—H22B | 108.2 |
| C31—C30—C32 | 120.1 (5) | C26—C27—H27A | 109.3 |
| C32—C30—C26 | 115.1 (5) | C26—C27—H27B | 109.3 |
| C17—N4—Ni2 | 126.7 (4) | C28—C27—C26 | 111.5 (5) |
| C21—N4—Ni2 | 113.2 (4) | C28—C27—H27A | 109.3 |
| C21—N4—C17 | 119.9 (5) | C28—C27—H27B | 109.3 |
| C3—C2—C1 | 118.6 (4) | H27A—C27—H27B | 108.0 |
| C3—C2—H2B | 120.7 | C23—C29—H29A | 109.5 |
| C1—C2—H2B | 120.7 | C23—C29—H29B | 109.5 |
| H25A—C25—H25B | 107.9 | C23—C29—H29C | 109.5 |
| C24—C25—H25A | 109.2 | H29A—C29—H29B | 109.5 |
| C24—C25—H25B | 109.2 | H29A—C29—H29C | 109.5 |
| C24—C25—C26 | 112.1 (4) | H29B—C29—H29C | 109.5 |
| C26—C25—H25A | 109.2 | C18—C19—H19 | 118.5 |
| C26—C25—H25B | 109.2 | C18—C19—C20 | 123.0 (7) |
| N2—C7—C8 | 109.8 (3) | C20—C19—H19 | 118.5 |
| N2—C7—C12 | 112.5 (3) | C21—C20—H20 | 120.5 |
| N2—C7—C13 | 107.1 (3) | C19—C20—C21 | 119.0 (7) |
| C8—C7—C12 | 108.5 (3) | C19—C20—H20 | 120.5 |
| Ni1—N1—C5—C4 | −178.5 (3) | N4—C21—C20—C19 | 2.4 (9) |
| Ni1—N1—C5—C6 | 2.4 (4) | C2—C3—C4—C5 | −0.9 (7) |
| Ni1—N1—C1—C2 | 177.8 (3) | C25—C24—C23—N5 | −168.7 (4) |
| Ni1—N3—C8—C9 | 171.5 (3) | C25—C24—C23—C28 | −45.9 (6) |
| Ni1—N3—C8—C7 | −10.6 (5) | C25—C24—C23—C29 | 76.9 (6) |
| Ni1—N2—C7—C8 | −7.7 (4) | C25—C26—C27—C28 | 59.6 (6) |
| Ni1—N2—C7—C12 | −128.6 (3) | C7—N2—C6—C5 | −83.5 (4) |
| Ni1—N2—C7—C13 | 109.3 (4) | C7—C8—C9—C10 | 47.9 (5) |
| Ni1—N2—C6—C5 | 43.4 (4) | C7—C12—C11—C10 | −57.9 (5) |
| Ni2—N6—C24—C25 | 173.2 (4) | C4—C5—C6—N2 | 148.6 (4) |
| Ni2—N6—C24—C23 | −12.5 (6) | C4—C3—C2—C1 | 0.6 (7) |
| Ni2—N5—C23—C24 | −13.2 (5) | C24—C25—C26—C30 | 73.6 (6) |
| Ni2—N5—C23—C28 | −134.2 (4) | C24—C25—C26—C27 | −52.8 (6) |
| Ni2—N5—C23—C29 | 104.5 (5) | C24—C23—C28—C27 | 49.5 (6) |
| Ni2—N5—C22—C21 | 44.6 (5) | C6—N2—C7—C8 | 114.5 (4) |
| Ni2—N4—C17—C18 | 174.2 (4) | C6—N2—C7—C12 | −6.5 (5) |
| Ni2—N4—C21—C22 | 5.4 (6) | C6—N2—C7—C13 | −128.6 (4) |
| Ni2—N4—C21—C20 | −178.0 (4) | C6—C5—C4—C3 | 180.0 (4) |
| O1—N3—C8—C9 | −0.7 (6) | C23—N5—C22—C21 | −79.6 (6) |
| O1—N3—C8—C7 | 177.3 (3) | C23—C28—C27—C26 | −59.7 (7) |
| N1—C5—C4—C3 | 1.0 (7) | C15—C14—C10—C9 | −24.5 (7) |
| N1—C5—C6—N2 | −32.3 (5) | C15—C14—C10—C11 | 101.6 (6) |
| N1—C1—C2—C3 | −0.2 (7) | C31—C30—C26—C25 | −6.7 (8) |
| N3—C8—C9—C10 | −134.2 (4) | C31—C30—C26—C27 | 117.5 (6) |
| N3—C8—C7—N2 | 11.5 (5) | C11—C12—C7—N2 | 172.3 (3) |
| N3—C8—C7—C12 | 134.8 (4) | C11—C12—C7—C8 | 50.6 (4) |
| N3—C8—C7—C13 | −104.9 (4) | C11—C12—C7—C13 | −67.8 (5) |
| O2—N6—C24—C25 | 1.3 (6) | C16—C14—C10—C9 | 158.2 (4) |
| O2—N6—C24—C23 | 175.6 (4) | C16—C14—C10—C11 | −75.7 (5) |
| C8—C9—C10—C14 | 77.6 (5) | C18—C19—C20—C21 | 1.5 (12) |
| C8—C9—C10—C11 | −49.1 (5) | C17—N4—C21—C22 | −179.7 (5) |
| C5—N1—C1—C2 | 0.3 (6) | C17—N4—C21—C20 | −3.0 (7) |
| N6—C24—C23—N5 | 16.7 (6) | C17—C18—C19—C20 | −4.4 (11) |
| N6—C24—C23—C28 | 139.5 (5) | C26—C25—C24—N6 | −136.7 (5) |
| N6—C24—C23—C29 | −97.7 (5) | C26—C25—C24—C23 | 49.2 (7) |
| N5—C23—C28—C27 | 170.8 (5) | C21—N4—C17—C18 | 0.0 (8) |
| C14—C10—C11—C12 | −72.9 (5) | C32—C30—C26—C25 | 174.8 (6) |
| C9—C8—C7—N2 | −170.4 (3) | C32—C30—C26—C27 | −60.9 (7) |
| C9—C8—C7—C12 | −47.1 (5) | C22—N5—C23—C24 | 106.3 (6) |
| C9—C8—C7—C13 | 73.2 (5) | C22—N5—C23—C28 | −14.6 (6) |
| C9—C10—C11—C12 | 55.6 (5) | C22—N5—C23—C29 | −135.9 (6) |
| C1—N1—C5—C4 | −0.6 (6) | C22—C21—C20—C19 | 178.6 (6) |
| C1—N1—C5—C6 | −179.7 (4) | C29—C23—C28—C27 | −72.1 (7) |
| C30—C26—C27—C28 | −67.9 (6) | C19—C18—C17—N4 | 3.8 (9) |
| N4—C21—C22—N5 | −35.0 (7) | C20—C21—C22—N5 | 148.7 (6) |