| Rigaku R-AXIS RAPIDII diffractometer | 3913 reflections with I > 2σ(I) |
| Detector resolution: 10.000 pixels mm-1 | Rint = 0.022 |
| ω scans | θmax = 30.0°, θmin = 3.0° |
| Absorption correction: numerical (NUMABS; Higashi, 1999) | h = −22→22 |
| Tmin = 0.916, Tmax = 0.968 | k = −10→10 |
| 29037 measured reflections | l = −35→35 |
| 4457 independent reflections |