| Rigaku R-AXIS RAPIDII diffractometer | 2563 reflections with I > 2σ(I) |
| Detector resolution: 10.000 pixels mm-1 | Rint = 0.038 |
| ω scans | θmax = 30.0°, θmin = 3.0° |
| Absorption correction: numerical (NUMABS; Higashi, 1999) | h = −9→10 |
| Tmin = 0.938, Tmax = 0.986 | k = −13→13 |
| 14544 measured reflections | l = −15→15 |
| 4486 independent reflections |
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