| Rigaku R-AXIS RAPIDII diffractometer | 3822 reflections with I > 2σ(I) |
| Detector resolution: 10.000 pixels mm-1 | Rint = 0.043 |
| ω scans | θmax = 30.0°, θmin = 3.2° |
| Absorption correction: numerical (NUMABS; Higashi, 1999) | h = −12→12 |
| Tmin = 0.868, Tmax = 0.915 | k = −13→13 |
| 22243 measured reflections | l = −14→14 |
| 4404 independent reflections |