| Rigaku R-AXIS RAPIDII diffractometer | 3854 reflections with I > 2σ(I) |
| Detector resolution: 10.000 pixels mm-1 | Rint = 0.022 |
| ω scans | θmax = 30.0°, θmin = 3.1° |
| Absorption correction: numerical (NUMABS; Higashi, 1999) | h = −9→9 |
| Tmin = 0.909, Tmax = 0.935 | k = −32→32 |
| 32362 measured reflections | l = −14→14 |
| 4588 independent reflections |