| Rigaku R-AXIS RAPIDII diffractometer | 3290 reflections with I > 2σ(I) |
| Detector resolution: 10.000 pixels mm-1 | Rint = 0.027 |
| ω scans | θmax = 27.5°, θmin = 3.1° |
| Absorption correction: numerical (NUMABS; Higashi, 1999) | h = −9→9 |
| Tmin = 0.868, Tmax = 0.960 | k = −10→10 |
| 18635 measured reflections | l = −17→17 |
| 3566 independent reflections |
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