Table 2. Experimental details.
| Crystal data | |
| Chemical formula | C16H17NO |
| M r | 239.30 |
| Crystal system, space group | Orthorhombic, P b c a |
| Temperature (K) | 296 |
| a, b, c (Å) | 7.6699 (4), 11.6080 (6), 30.1431 (17) |
| V (Å3) | 2683.7 (2) |
| Z | 8 |
| Radiation type | Mo Kα |
| μ (mm−1) | 0.07 |
| Crystal size (mm) | 0.68 × 0.48 × 0.18 |
| Data collection | |
| Diffractometer | Stoe IPDS 2 |
| Absorption correction | Integration (X-RED32; Stoe & Cie, 2002 ▸) |
| T min, T max | 0.953, 0.990 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 14869, 2213, 1451 |
| R int | 0.081 |
| (sin θ/λ)max (Å−1) | 0.583 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.042, 0.125, 1.00 |
| No. of reflections | 2213 |
| No. of parameters | 168 |
| H-atom treatment | H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) | 0.11, −0.11 |