Table 6.
13C-NMR data of the sugar portion of compounds 6–10.
Sugars | Compounds | ||||
---|---|---|---|---|---|
Ara(p) | 6 b | 7 a | 8 a | 9 a | 10 a |
1 | 101.31 | 101.61 | 101.53 | 101.64 | 101.26 |
2 | 74.21 | 74.46 | 74.58 | 74.51 | 74.28 |
3 | 85.32 | 85.37 | 85.42 | 71.21 | 85.32 |
4 | 70.24 | 69.96 | 70.65 | 85.37 | 70.54 |
5 | 67.58 | 67.18 | 67.17 | 67.04 | 67.08 |
Rha | |||||
1 | 102.02 | 101.47 | 101.69 | 101.47 | 101.71 |
2 | 72.39 | 71.96 | 72.00 | 71.98 | 72.38 |
3 | 80.40 | 80.46 | 80.48 | 80.46 | 72.12 |
4 | 73.17 | 73.01 | 73.06 | 73.03 | 74.42 |
5 | 70.13 | 69.80 | 69.84 | 69.81 | 69.87 |
6 | 19.63 | 18.73 | 18.72 | 18.73 | 18.64 |
Xyl | |||||
1 | 107.16 | 106.50 | 106.54 | 106.52 | 106.49 |
2 | 75.23 | 74.88 | 74.92 | 74.90 | 74.90 |
3 | 78.95 | 78.05 | 78.09 | 78.05 | 77.99 |
4 | 71.59 | 71.19 | 71.23 | 70.65 | 70.73 |
5 | 67.58 | 67.02 | 67.04 | 68.18 | 67.02 |
Api | |||||
1 | 112.31 | 112.13 | 112.18 | 112.16 | 101.26 |
2 | 78.36 | 78.24 | 78.27 | 78.25 | 74.28 |
3 | 80.83 | 80.48 | 80.48 | 80.48 | 85.32 |
4 | 75.73 | 75.16 | 75.18 | 75.18 | 70.54 |
5 | 66.17 | 65.56 | 65.59 | 65.59 | 67.08 |
a Tested in CD3OD; b tested in C5D5N.