Skip to main content
. 2021 Nov 8;26(21):6754. doi: 10.3390/molecules26216754

Table 2.

Composition of lignin obtained with each organosolv pretreatment. Weight average (MW), number-average (Mn), and polydispersity index (PDI) of acid-insoluble lignin from birch sawdust were determined after acetobromination.

Code Cellulose (%) Hemicellulose (%) Klason Lignin (%) Ash (%) MW (g/mol) Mn (g/mol) PDI
B0A5a 0.08 1.85 95.18 0.47 4500 1200 3.75
B0A6a 0.14 2.32 83.86 0.27 8000 1100 7.34
B0A6c 0.50 0.32 86.44 0.42 9700 1400 6.97
B0B5a 0.39 1.56 92.00 0.72 11300 1400 8.21
B0B6a 0.00 2.01 91.90 0.31 13300 1700 8.04
B1A5a 0.14 3.55 77.93 0.12 1800 800 2.28
B1A6a 0.18 7.04 74.27 0.21 4500 1200 3.87
B1B5a 0.10 2.48 83.08 0.11 4600 1200 3.88
B1B6a 0.11 3.25 89.05 0.08 15900 1900 8.53

Representation of the codes: 0—pretreatment at 200 °C; 1—pretreatment at 180 °C; A—pretreatment time of 15 min; B—pretreatment of 30 min; 5—50% v/v ethanol content; 6—60% v/v ethanol content; a—no catalyst added; c—1% w/wbiomass H2SO4.