Table 3.
Data collectiona and refinement statistics
| REV1 UBM2/Ub | |
|---|---|
| Data Collection | |
| Space group | I432 |
| Cell dimensions | |
| a, b, c (Å) | 164.9 |
| α, β,γ (°) | 90.0 |
| Resolution (Å) | 2.35 (2.39–2.35)b |
| Rsym (%) | 10.6 (53.2) |
| Rmeas (%) | 11.4 (59.3) |
| Rpim (%) | 4.2 (25.5) |
| I/σ | 15.9 (2.2) |
| Completeness (%) | 99.1 (100.0) |
| Redundancy | 6.9 (5.0) |
| Refinement | |
| Resolution (A) | 30.0–2.35 |
| No. reflections | 16,000 |
| Rwork / Rfree (%) | 20.1/22.9 |
| No. atoms | |
| Protein | 1,476 |
| Ions | 4 |
| Water | 73 |
| B-factors | |
| Protein | 38.7 |
| Ions | 38.4 |
| Water | 40.2 |
| R.m.s. deviations | |
| Bond lengths(Å) | 0.006 |
| Bond angles (°) | 0.5 |
| Ramachandran Plot Statisticsc (%) | |
| Preferred regions | 98.4 |
| Allowed regions | 1.6 |
a
Dataset was collected from a single crystal.
b
Values in parenthesis are for the highest resolution shell
c
As defined by Molprobity