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. 2021 Nov 25;12:6908. doi: 10.1038/s41467-021-27282-9

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© The Author(s) 2021

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Fig. 2 — a TG curve of compound 1-0D with a heating rate of 3 K min⁻¹. The weight losses of 18% at 380 K and 36% at 410 K suggest that two-thirds of the eg ligands are eliminated in the two-step transformation upon heating. b Variable-temperature PXRD of 1-0D. The peaks corresponding to 1-1D and 1-3D appear at 343 and 378 K, respectively.