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. 2021 Nov 10;33(22):8693–8704. doi: 10.1021/acs.chemmater.1c02654

Table 1. Summary of Synthesis Conditions and Samples Features Drying time of the FeOl Precursor Prior to NP Synthesis, Volumes of 1-Octadecene and Dibenzyl Ether (ODE:DBE) Used in the NP Synthesis, The Molar Ratio of Oleic Acid and FeOl (O.A:FeOl), Final Temperature, Reflux Time, Crystallite Size (DXRD) Calculated by the Scherrer Equation, Particle Mean Dimension Obtained by TEM (DTEM), and Saturation Magnetization (Ms) at RT. The Three Optimization Stages are: Opt1, Opt2, and Opt3 (Arranged in Increasing Gray Levels).

2.1.

a

Samples from ref (27). Opt1-48 was mechanically stirred at 60 rpm and the rest of the samples at 120 rpm.

b

Samples from ref (29).

c

Opt3 batch. The reaction vessel was completely sealed up using adjustable homemade ground glass joint clips.