Table 1.

EDX analysis of the synthesized five alloys equipped with TEM and SEM. Reaction reference: 0.1 M metal concentration, 80 mL reaction volume, 1400 rpm, and 95–98 °C.

Iron: Nickel Molar Ratio	TEM EDX Analysis						SEM EDX Analysis
	Atomic %			Mass %			Atomic %			Mass %
	Fe	Ni	O	Fe	Ni	O	Fe	Ni	O	Fe	Ni	O
10:90	11.36	88.64	0.00	10.87	89.13	0.00	10.74	89.22	0.05	10.27	89.72	0.01
20:80	17.50	71.71	10.78	18.24	78.54	3.22	20.05	79.05	0.89	19.39	80.36	0.25
30:70	28.51	62.44	9.06	29.47	67.85	2.68	31.25	67.22	1.53	30.53	69.04	0.43
40:60	34.88	47.76	17.36	38.73	55.75	5.52	39.89	56.60	3.51	39.20	58.27	2.53
50:50	39.06	40.19	20.74	44.77	48.42	6.81	41.92	42.82	15.26	45.91	49.30	4.79