Table 3. Experimental details.
| Crystal data | |
| Chemical formula | [Sb3Te(C6H5)9O6] |
| M r | 1282.75 |
| Crystal system, space group | Monoclinic, C2/c |
| Temperature (K) | 173 |
| a, b, c (Å) | 47.714 (2), 9.1176 (4), 22.9324 (10) |
| β (°) | 104.168 (4) |
| V (Å3) | 9672.9 (8) |
| Z | 8 |
| Radiation type | Mo Kα |
| μ (mm−1) | 2.31 |
| Crystal size (mm) | 0.28 × 0.22 × 0.21 |
| Data collection | |
| Diffractometer | Stoe IPDS |
| Absorption correction | Numerical [X-RED (Stoe & Cie, 2001 ▸) and X-SHAPE (Stoe & Cie, 1999 ▸)] |
| T min, T max | 0.499, 0.572 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 29796, 10754, 8356 |
| R int | 0.053 |
| (sin θ/λ)max (Å−1) | 0.644 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.038, 0.096, 0.93 |
| No. of reflections | 10754 |
| No. of parameters | 577 |
| H-atom treatment | H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) | 1.00, −1.24 |