Table 2. Synthesis of SIAs from PFAA and SAsa.
Reaction conditions: PFAA (0.3–0.9 mmol, 0.05 M), SA (0.45–1.35 mmol, 1.5 equiv), degassed PhCF3, 390 nm Kessil LED light, 2–16 h, r.t.
Average yield of two syntheses.
From the racemic starting material.