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. 2021 Nov 12;86(23):17119–17128. doi: 10.1021/acs.joc.1c02241

Table 2. Synthesis of SIAs from PFAA and SAsa.

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a

Reaction conditions: PFAA (0.3–0.9 mmol, 0.05 M), SA (0.45–1.35 mmol, 1.5 equiv), degassed PhCF3, 390 nm Kessil LED light, 2–16 h, r.t.

b

Average yield of two syntheses.

c

From the racemic starting material.