Table 4.
Robustness study data
| Method | Parameter | Value | Tailing factor | Number of theoretical plates | Content (%) |
|---|---|---|---|---|---|
| Liquid Chromatographic method | Acetonitrile composition% | 9 | 0.775 | 11 824 | 100.15 |
| 11 | 0.739 | 11 789 | 99.87 | ||
| Flow rate (mL min-1) |
0.9 | 0.753 | 11 624 | 99.78 | |
| 1.1 | 0.746 | 11 698 | 100.02 | ||
| Spectrophotometric method |
Solvent | Methanol | 100.25 | ||
| Ethanol | 99.74 | ||||
| Isopropyl alcohol | 100.03 | ||||
| Detection wavelengths | 225 | 99.94 | |||
| 229 | 100.14 |