Table 4. Stability Study Data for the Quantification of Rottlerin in Plasmaa.
stability study | measured concentration (ng/mL) | accuracy (%) | % CV |
---|---|---|---|
LQC | |||
0 h | 5.46 | 95.70 | 1.08 |
short-term | 5.89 | 91.05 | 3.11 |
autosampler | 5.13 | 90.04 | 2.72 |
freeze–thaw | 5.05 | 88.60 | 3.31 |
long-term | 5.19 | 103.25 | 2.37 |
HQC | |||
0 h | 755.16 | 94.40 | 0.55 |
short-term | 760.43 | 93.85 | 1.19 |
autosampler | 743.15 | 92.89 | 2.09 |
freeze–thaw | 733.56 | 91.69 | 1.05 |
long-term | 750.80 | 95.05 | 1.96 |
5.7 ng/mL (LQC) and 800 ng/mL (HQC); n = 4 for each QC level in individual stability study data.