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| entry | solvent | solvent (V) | % mass recoverya | wt % purityb |
|---|---|---|---|---|
| 1 | chlorobenzene | 10 | 53 | 98 |
| 2 | CPME | 10 | 23 | 97 |
| 3 | anisole | 10 | 30 | 69 |
| 4 | toluene/chlorobenzene (1:1) | 5 | 61 | 96 |
| 5 | toluene | 10 | 84 | 82 |
| 6 | i-PrOAc | 2.5 | 66 | 98 |
| 7 | CH3CN | 2.5 | 64 | 96 |
Adjusted to purity.
By qNMR.
