Skip to main content
. Author manuscript; available in PMC: 2022 Nov 15.
Published in final edited form as: J Am Chem Soc. 2021 Oct 28;143(44):18617–18625. doi: 10.1021/jacs.1c08551

Figure 1.

Figure 1.

Oxidative addition and carbonyl de-insertion of TFAAn at SPhos/Pd0 in THF. 19F NMR spectra of (A) TFAAn; (B) Reaction of TFAAn with SPhos/Pd0 in THF after 0.25 h at room temperature; (C) Reaction of TFAAn with SPhos/Pd0 in THF after 4 h at room temperature; (D) Reaction heated to 90°C for 0.5 h. Spectra are referenced to 4-fluorotoluene (−119.85 ppm).