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. Author manuscript; available in PMC: 2022 Nov 15.
Published in final edited form as: J Am Chem Soc. 2021 Oct 28;143(44):18617–18625. doi: 10.1021/jacs.1c08551

Figure 2.

Figure 2.

Oxidative addition and carbonyl de-insertion of DFAAn at SPhos/Pd0 in THF. 19F NMR spectrum of (A) DFAAn; (B) Reaction of DFAAn with SPhos/Pd0 in THF after 15 min at room temperature; (C) Reaction of DFAAn with SPhos/Pd0 in THF after 10 h at room temperature. Black star represents 4-fluorotoluene (−119.85 ppm, internal standard).