13C NMR spectroscopic data of compounds 1–6 (100 MHz, CDCl3, δ in ppm).
| Position | 1 | 2 | 3 | 4 | 5 | 6 |
|---|---|---|---|---|---|---|
| 1 | 195.6 | 193.2 | 192.6 | 193.8 | — | 110.1 |
| 2 | 110.3 | 113.3 | 112.7 | 110.7 | 171.3 | 161.2 |
| 3 | 197.9 | 196.5 | 195.8 | 196.3 | 108.4 | 108.4 |
| 4 | 31.3 | 42.0 | 41.4 | 38.4 | 183.6 | 135.6 |
| 5 | 26.9 | 63.9 | 63.3 | 67.0 | 160.8 | 108.4 |
| 6 | 71.3 | 47.7 | 47.0 | 74.7 | 111.1 | 161.2 |
| 7 | — | — | — | — | 135.0 | — |
| 8 | — | — | — | — | 106.9 | — |
| 9 | — | — | — | — | 156.8 | — |
| 10 | — | — | — | — | 110.6 | — |
| 1′ | 206.1 | 206.1 | 205.4 | 205.4 | 34.4 | 208.0 |
| 2′ | 40.3 | 40.8 | 40.1 | 40.2 | 26.8 | 44.8 |
| 3′ | 24.6 | 25.1 | 31.6–29.2 | 25.1 | 29.8–29.0 | 24.4 |
| 4′–8′ | 29.8–29.3 | 30.2–29.8 | 31.6–29.2 | 30.2–29.8 | 29.8–29.0 | 29.8–29.3 |
| 9′ | 29.8–29.3 | 30.2–29.8 | 31.6–29.2 | 30.2–29.8 | 27.2 | 29.8–29.3 |
| 10′ | 29.8–29.3 | 30.2–29.8 | 31.6–29.2 | 30.2–29.8 | 129.9 | 29.8–29.3 |
| 11′ | 29.8–29.3 | 30.2–29.8 | 35.5 | 30.2–29.8 | 129.9 | 29.8–29.3 |
| 12′ | 27.2 | 27.7 | 136.7 | 27.7 | 27.2 | 27.2 |
| 13′ | 129.9 | 130.4 | 108.7 | 130.4 | 32.0 | 129.9 |
| 14′ | 129.9 | 130.4 | 147.2 | 130.4 | 22.4 | 129.9 |
| 15′ | 27.2 | 27.4 | 145.2 | 27.4 | 14.1 | 26.9 |
| 16′ | 32.0 | 32.4 | 107.8 | 32.4 | — | 32.0 |
| 17′ | 22.4 | 22.8 | 120.8 | 22.8 | — | 22.4 |
| 18′ | 14.0 | 14.5 | — | 14.5 | — | 14.0 |
| OCH2O | — | — | 100.5 | — | — | — |