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. 2021 Jan 20;11(7):4097–4103. doi: 10.1039/d0ra10498a

13C NMR spectroscopic data of compounds 1–6 (100 MHz, CDCl3, δ in ppm).

Position 1 2 3 4 5 6
1 195.6 193.2 192.6 193.8 110.1
2 110.3 113.3 112.7 110.7 171.3 161.2
3 197.9 196.5 195.8 196.3 108.4 108.4
4 31.3 42.0 41.4 38.4 183.6 135.6
5 26.9 63.9 63.3 67.0 160.8 108.4
6 71.3 47.7 47.0 74.7 111.1 161.2
7 135.0
8 106.9
9 156.8
10 110.6
1′ 206.1 206.1 205.4 205.4 34.4 208.0
2′ 40.3 40.8 40.1 40.2 26.8 44.8
3′ 24.6 25.1 31.6–29.2 25.1 29.8–29.0 24.4
4′–8′ 29.8–29.3 30.2–29.8 31.6–29.2 30.2–29.8 29.8–29.0 29.8–29.3
9′ 29.8–29.3 30.2–29.8 31.6–29.2 30.2–29.8 27.2 29.8–29.3
10′ 29.8–29.3 30.2–29.8 31.6–29.2 30.2–29.8 129.9 29.8–29.3
11′ 29.8–29.3 30.2–29.8 35.5 30.2–29.8 129.9 29.8–29.3
12′ 27.2 27.7 136.7 27.7 27.2 27.2
13′ 129.9 130.4 108.7 130.4 32.0 129.9
14′ 129.9 130.4 147.2 130.4 22.4 129.9
15′ 27.2 27.4 145.2 27.4 14.1 26.9
16′ 32.0 32.4 107.8 32.4 32.0
17′ 22.4 22.8 120.8 22.8 22.4
18′ 14.0 14.5 14.5 14.0
OCH2O 100.5