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. 2021 Feb 10;11(12):6662–6666. doi: 10.1039/d0ra10068d

The results of synthesizing 3a–3gvia the irradiation of 2a–2g in HCl/DMF at 365 nm.

En. Starting Conv. (%) Yield (%) based on conversion Yield of 3 (%) 3-Step yield (%)
1 2a: H 82 97 79.54 72.47
2 2b: Me 61 95 57.95 51.15
3 2c: Et 65 98 63.7 54.99
4 2d: i-Pr 74 98 72.52 62.72
5 2e: F 72 98 70.56 60.29
6 2f: Cl 76 97 73.72 65.74
7 2g: Br 77 96 73.92 68.06