The results of synthesizing 3a–3gvia the irradiation of 2a–2g in HCl/DMF at 365 nm.
| En. | Starting | Conv. (%) | Yield (%) based on conversion | Yield of 3 (%) | 3-Step yield (%) |
|---|---|---|---|---|---|
| 1 | 2a: H | 82 | 97 | 79.54 | 72.47 |
| 2 | 2b: Me | 61 | 95 | 57.95 | 51.15 |
| 3 | 2c: Et | 65 | 98 | 63.7 | 54.99 |
| 4 | 2d: i-Pr | 74 | 98 | 72.52 | 62.72 |
| 5 | 2e: F | 72 | 98 | 70.56 | 60.29 |
| 6 | 2f: Cl | 76 | 97 | 73.72 | 65.74 |
| 7 | 2g: Br | 77 | 96 | 73.92 | 68.06 |