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. 2021 Feb 10;11(12):6662–6666. doi: 10.1039/d0ra10068d

Results of the synthesis of 4a–4gvia the irradiation of 2a–2g in HCl/acetal at 419 nm.

En. Starting Conv. (%) Yield (%) based on conversion Yield of 4 (%) 3-Step yield (%)
1 2a: H 93 96 89.28 81.37
2 2b: Me 76 86 65.36 57.69
3 2c: Et 75 86 64.50 55.68
4 2d: i-Pr 72 73 52.56 45.45
5 2e: F 67 91 60.97 52.09
6 2f: Cl 66 91 60.06 53.56
7 2g: Br 77 90 69.30 63.80