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. 2021 Nov 24;6(50):34501–34511. doi: 10.1021/acsomega.1c04741

Table 4. Nonlinear Effect Experiment.

entry 1 2 3 4 5 6 7
ee of cat 1k (%) 0 20 40 50 60 80 100
ee of product (%)b 0 18 37 49 55 73 92
yield (5)a 89 90 91 90 87 93 98
a

Yield of isolated products.

b

Determined by the GC HP-1 column (30 m × 0.32 mm × 0.25 μm). Conditions: initial temperature, 50 °C; initial time, 3 min; 25.0 °C/min; final temperature, 280 °C; 17 psi; retention time, 10.76, 14.12 min.