Table 20.
C | 1 | 2 | 3 | 4 | 5 | 7 | 11 | 13 | 14 |
---|---|---|---|---|---|---|---|---|---|
2 | 161.2 | 147.4 | 147.7 | 147.8 | 147.4 | 167.2 | 167.8 | 158.6 | 159.5 |
3 | 93.1 | 141.2 | 141.0 | 138.1 | 141.5 | 111.7 | 109.1 | 112.0 | 112.8 |
4 | 166.6 | 178.4 | 178.5 | 177.0 | 178.4 | 180.3 | 183.2 | 183.6 | 184.4 |
5 | 137.1 | 163.4 | 163.3 | 161.5 | 163.4 | 160.2 | 93.9 | 163.4 | 163.9 |
6 | 132.0 | 100.1 | 100.2 | 98.8 | 100.2 | 104.6 | 162.0 | 101.3 | 101.9 |
7 | 127.8 | 166.4 | 166.3 | 164.3 | 166.5 | 164.7 | 110.2 | 164.9 | 165.2 |
8 | 114.9 | 95.0 | 95.0 | 93.8 | 95.0 | 99.1 | 159.6 | 96.2 | 96.9 |
9 | 154.3 | 159.3 | 159.3 | 157.2 | 159.4 | 161.1 | 156.6 | 159.5 | 160.2 |
10 | 114.5 | 106.2 | 106.2 | 104.8 | 106.1 | 109.2 | 106.1 | 108.4 | 109.3 |
11 | 23.2 | - | - | - | - | 19.9 | 20.3 | - | - |
12 | - | - | - | - | - | - | 8.2 | - | - |
1′ | 100.1 | 104.6 | 104.4 | 100.6 | 104.2 | 105.0 | 101.7 | 101.6 | 102.1 |
2′ | 73.2 | 74.6 | 72.0 | 69.9 | 74.8 | 74.6 | 75.1 | 74.7 | 75.1 |
3′ | 77.5 | 77.1 | 73.6 | 70.2 | 77.4 | 77.3 | 78.4 | 77.9 | 77.8 |
4′ | 69.6 | 70.8 | 69.2 | 71.5 | 71.3 | 71.3 | 80.5 | 71.2 | 73.9 |
5′ | 76.7 | 67.1 | 67.1 | 69.7 | 78.5 | 78.7 | 78.1 | 78.4 | 77.5 |
6′ | 60.7 | - | - | 17.7 | 62.6 | 62.5 | 60.9 | 62.4 | 171.5 |
OCH3 | - | - | - | - | - | - | - | - | 53.8 |
Solvent | DMSO-d6 | CD3OD | CD3OD | DMSO-d6 | CD3OD | CD3OD | C5D5N | CD3OD | CD3OD |
References | [7] | [10] | [12] | [9] | [11] | [17] | [1] | [27] | [28] |