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. 2021 Dec 16;26(24):7646. doi: 10.3390/molecules26247646

Table 20.

The 13C-NMR spectral data of compounds 114 except those which have no reported 13C-NMR data.

C 1 2 3 4 5 7 11 13 14
2 161.2 147.4 147.7 147.8 147.4 167.2 167.8 158.6 159.5
3 93.1 141.2 141.0 138.1 141.5 111.7 109.1 112.0 112.8
4 166.6 178.4 178.5 177.0 178.4 180.3 183.2 183.6 184.4
5 137.1 163.4 163.3 161.5 163.4 160.2 93.9 163.4 163.9
6 132.0 100.1 100.2 98.8 100.2 104.6 162.0 101.3 101.9
7 127.8 166.4 166.3 164.3 166.5 164.7 110.2 164.9 165.2
8 114.9 95.0 95.0 93.8 95.0 99.1 159.6 96.2 96.9
9 154.3 159.3 159.3 157.2 159.4 161.1 156.6 159.5 160.2
10 114.5 106.2 106.2 104.8 106.1 109.2 106.1 108.4 109.3
11 23.2 - - - - 19.9 20.3 - -
12 - - - - - - 8.2 - -
1′ 100.1 104.6 104.4 100.6 104.2 105.0 101.7 101.6 102.1
2′ 73.2 74.6 72.0 69.9 74.8 74.6 75.1 74.7 75.1
3′ 77.5 77.1 73.6 70.2 77.4 77.3 78.4 77.9 77.8
4′ 69.6 70.8 69.2 71.5 71.3 71.3 80.5 71.2 73.9
5′ 76.7 67.1 67.1 69.7 78.5 78.7 78.1 78.4 77.5
6′ 60.7 - - 17.7 62.6 62.5 60.9 62.4 171.5
OCH3 - - - - - - - - 53.8
Solvent DMSO-d6 CD3OD CD3OD DMSO-d6 CD3OD CD3OD C5D5N CD3OD CD3OD
References [7] [10] [12] [9] [11] [17] [1] [27] [28]