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. 2021 Dec 16;26(24):7646. doi: 10.3390/molecules26247646

Table 21.

The 13C-NMR spectral data of compounds 1523 except which has no reported 13C-NMR data.

C 15 16 17 18 20 21 22 23
2 158.1 158.4 158.5 168.9 161.6 174.3 175.5 174.6
3 110.8 111.9 112.0 108.8 108.8 107.8 106.2 106.6
4 181.8 183.6 183.6 182.5 182.5 184.3 183.3 183.1
5 161.3 163.1 163.2 161.2 157.9 163.0 162.2 162.7
6 99.8 101.2 101.2 99.8 100.3 101.0 100.6 100.7
7 162.9 164.6 164.8 163.1 168.9 164.8 164.2 164.2
8 94.6 96.2 96.2 94.9 95.0 95.9 95.3 95.3
9 157.7 159.4 159.4 157.9 163.4 159.5 158.4 158.4
10 106.8 108.5 108.5 105.5 105.5 107.0 106.5 107.4
11 - - - 20.5 20.5 28.3 33.3 40.4
12 - - - - - 11.2 19.9 27.6
13 - - - - - - 19.9 17.7
14 - - - - - - - 11.7
1′ 99.7 101.5 101.5 100.6 99.9 101.6 101.7 101.7
2′ 73.1 74.7 74.7 73.3 73.5 74.7 74.8 74.8
3′ 76.2 77.9 77.9 76.6 77.6 77.8 78.5 78.5
4′ 69.7 71.9 72.0 69.6 70.7 71.2 71.2 71.1
5′ 74.1 75.8 76.0 66.2 76.8 78.4 79.3 79.2
6′ 63.4 64.2 64.7 - 61.1 62.4 62.4 62.3
1″ 119.5 127.4 127.3 - - - - -
2″ 108.8 133.7 131.2 - - - - -
3″ 145.6 115.8 117.0 - - - - -
4″ 138.6 160.0 161.4 - - - - -
5″ 145.6 115.8 117.0 - - - - -
6″ 108.8 133.7 131.2 - - - - -
7″ 165.9 145.1 146.9 - - - - -
8″ - 116.0 115.1 - - - - -
9″ - 168.1 168.9 - - - - -
Solvent DMSO-d6 CD3OD CD3OD DMSO-d6 DMSO-d6 CD3OD C5D5N C5D5N
References [29] [30] [30] [31] [157] [40] [41] [41]