Table 21.
C | 15 | 16 | 17 | 18 | 20 | 21 | 22 | 23 |
---|---|---|---|---|---|---|---|---|
2 | 158.1 | 158.4 | 158.5 | 168.9 | 161.6 | 174.3 | 175.5 | 174.6 |
3 | 110.8 | 111.9 | 112.0 | 108.8 | 108.8 | 107.8 | 106.2 | 106.6 |
4 | 181.8 | 183.6 | 183.6 | 182.5 | 182.5 | 184.3 | 183.3 | 183.1 |
5 | 161.3 | 163.1 | 163.2 | 161.2 | 157.9 | 163.0 | 162.2 | 162.7 |
6 | 99.8 | 101.2 | 101.2 | 99.8 | 100.3 | 101.0 | 100.6 | 100.7 |
7 | 162.9 | 164.6 | 164.8 | 163.1 | 168.9 | 164.8 | 164.2 | 164.2 |
8 | 94.6 | 96.2 | 96.2 | 94.9 | 95.0 | 95.9 | 95.3 | 95.3 |
9 | 157.7 | 159.4 | 159.4 | 157.9 | 163.4 | 159.5 | 158.4 | 158.4 |
10 | 106.8 | 108.5 | 108.5 | 105.5 | 105.5 | 107.0 | 106.5 | 107.4 |
11 | - | - | - | 20.5 | 20.5 | 28.3 | 33.3 | 40.4 |
12 | - | - | - | - | - | 11.2 | 19.9 | 27.6 |
13 | - | - | - | - | - | - | 19.9 | 17.7 |
14 | - | - | - | - | - | - | - | 11.7 |
1′ | 99.7 | 101.5 | 101.5 | 100.6 | 99.9 | 101.6 | 101.7 | 101.7 |
2′ | 73.1 | 74.7 | 74.7 | 73.3 | 73.5 | 74.7 | 74.8 | 74.8 |
3′ | 76.2 | 77.9 | 77.9 | 76.6 | 77.6 | 77.8 | 78.5 | 78.5 |
4′ | 69.7 | 71.9 | 72.0 | 69.6 | 70.7 | 71.2 | 71.2 | 71.1 |
5′ | 74.1 | 75.8 | 76.0 | 66.2 | 76.8 | 78.4 | 79.3 | 79.2 |
6′ | 63.4 | 64.2 | 64.7 | - | 61.1 | 62.4 | 62.4 | 62.3 |
1″ | 119.5 | 127.4 | 127.3 | - | - | - | - | - |
2″ | 108.8 | 133.7 | 131.2 | - | - | - | - | - |
3″ | 145.6 | 115.8 | 117.0 | - | - | - | - | - |
4″ | 138.6 | 160.0 | 161.4 | - | - | - | - | - |
5″ | 145.6 | 115.8 | 117.0 | - | - | - | - | - |
6″ | 108.8 | 133.7 | 131.2 | - | - | - | - | - |
7″ | 165.9 | 145.1 | 146.9 | - | - | - | - | - |
8″ | - | 116.0 | 115.1 | - | - | - | - | - |
9″ | - | 168.1 | 168.9 | - | - | - | - | - |
Solvent | DMSO-d6 | CD3OD | CD3OD | DMSO-d6 | DMSO-d6 | CD3OD | C5D5N | C5D5N |
References | [29] | [30] | [30] | [31] | [157] | [40] | [41] | [41] |