Table 22.
C | 24 | 25 | 26 | 28 | 29 | 30 | 31 | 32 |
---|---|---|---|---|---|---|---|---|
2 | 168.7 | 157.3 | 167.9 | 168.2 | 168.9 | 169.2 | 168.9 | 168.5 |
3 | 108.7 | 108.3 | 108.8 | 108.8 | 108.8 | 109.3 | 108.8 | 108.4 |
4 | 182.4 | 181.9 | 182.7 | 182.8 | 182.5 | 184.2 | 182.5 | 182.1 |
5 | 161.5 | 161.1 | 162.4 | 162.4 | 161.7 | 163.1 | 161.7 | 161.3 |
6 | 99.9 * | 108.7 | 100.6 | 100.7 | 100.2 | 100.8 | 100.0 | 99.6 |
7 | 162.9 | 162.6 | 163.9 | 163.9 | 161.9 | 163.4 | 161.9 | 161.6 |
8 | 94.9 | 108.2 | 95.3 | 95.1 | 95.2 | 95.7 | 95.1 | 94.7 |
9 | 157.7 | 168.2 | 158.3 | 158.3 | 157.9 | 159.5 | 157.9 | 157.5 |
10 | 105.5 | 105.0 | 106.3 | 106.3 | 105.7 | 106.8 | 105.6 | 105.2 |
11 | 20.3 | 19.9 | 19.9 | 20.1 | 20.5 | 20.4 | 20.5 | 20.1 |
1′ | 99.8 * | 99.3 | 101.9 | 102.0 | 98.8 | 99.6 | 98.5 | 98.1 |
2′ | 73.3 | 77.0 | 74.6 | 74.6 | 81.2 | 71.0 | 69.8 | 69.5 |
3′ | 76.5 | 75.8 | 78.5 | 78.5 | 70.4 | 82.5 | 82.1 | 70.3 |
4′ | 70.2 | 68.9 | 71.5 | 71.6 | 70.9 | 72.4 | 70.7 | 81.4 |
5′ | 74.1 | 76.0 | 77.4 | 77.5 | 69.4 | 70.9 | 68.7 | 68.5 |
6′ | 63.7 | 60.5 | 69.0 | 68.0 | 18.3 | 18.1 | 18.0 | 17.9 |
1″ | - | 108.7 | 111.2 | 102.7 | 105.0 | 105.9 | 104.8 | 104.4 |
2″ | - | 76.7 | 77.9 | 72.0 | 74.5 | 75.4 | 74.1 | 74.5 |
3″ | - | 79.2 | 80.3 | 72.8 | 77.2 | 77.8 | 76.8 | 77.1 |
4″ | - | 73.9 | 75.1 | 74.1 | 70.0 | 71.1 | 70.6 | 70.1 |
5″ | - | 64.1 | 65.8 | 69.8 | 76.7 | 77.7 | 74.8 | 76.7 |
6″ | - | - | - | 18.6 | 61.5 | 62.2 | 64.1 | 61.2 |
CH3CO | 20.9, 170.5 | - | - | - | - | - | 21.1, 170.6 | - |
Solvent | DMSO-d6 | CDCl3, DMSO-d6 | C5D5N | C5D5N | DMSO-d6 | DMSO-d6 | DMSO-d6 | DMSO-d6 |
References | [33] | [16] | [44] | [46] | [31] | [22] | [31] | [47] |
* Data interchangeable.