Table 24.
C | 43 | 45 | 46 | 47 | 48 | 49 | 50 | 52 |
---|---|---|---|---|---|---|---|---|
2 | 168.7 | 168.4 | 168.4 | 169.5 | 170.0 | 160.0 | 164.9 | 164.9 |
3 | 108.4 | 108.0 | 108.0 | 108.4 | 109.1 | 112.5 | 101.9 | 118.6 |
4 | 182.9 | 182.7 | 182.7 | 182.4 | 185.0 | 185.0 | 178.8 | 177.6 |
5 | 159.5 | 152.6 | 155.9 | 152.5 | 157.8 | 158.8 | 141.8 | 137.9 |
6 | 98.3 | 109.7 | 114.3 | 135.2 | 116.3 | 117.3 | 116.6 | 110.5 |
7 | 160.9 | 158.5 | 158.8 | 157.8 | 160.2 | 161.2 | 160.4 | 159.8 |
8 | 104.6 | 114.3 | 109.8 | 94.7 | 111.6 | 112.9 | 111.5 | 99.6 |
9 | 155.0 | 155.9 | 152.6 | 155.6 | 154.6 | 155.5 | 159.3 | 158.5 |
10 | 105.2 | 106.5 | 106.5 | 106.2 | 108.2 | 110.6 | 117.1 | 115.7 |
11 | 20.5 | 20.0 | 20.1 | 20.2 | 20.5 | 10.3 | 22.8 | 19.4 |
12 | 8.1 | 8.8 | 9.0 | - | 8.9 | 10.5 | 19.9 | 48.7 |
13 | - | 8.9 | 9.1 | - | 9.5 | - | - | 205.3 |
14 | - | - | - | - | - | - | - | 52.0 |
15 | - | - | - | - | - | - | - | 62.7 |
16 | - | - | - | - | - | - | - | 23.6 |
1′ | 100.3 | 104.3 | 104.4 | 100.8 | 105.7 | 106.5 | 100.3 | 102.1 |
2′ | 73.9 | 76.0 | 74.1 | 74.1 | 75.3 | 76.5 | 77.6 | 73.0 |
3′ | 76.5 | 73.9 | 76.3 | 78.0 | 75.6 | 78.5 | 73.6 | 76.3 |
4′ | 79.4 | 70.0 | 69.9 | 69.9 | 71.7 | 72.5 | 70.1 | 69.4 |
5′ | 76.1 | 73.4 | 77.0 | 77.0 | 77.7 | 76.4 | 76.9 | 77.0 |
6′ | 60.7 | 63.0 | 61.0 | 61.2 | 64.3 | 65.3 | 61.0 | 60.5 |
1″ | - | - | - | - | - | 173.1 | - | - |
2″ | - | - | - | - | - | 47.3 | - | - |
3″ | - | - | - | - | - | 71.4 | - | - |
4″ | - | - | - | - | - | 46.9 | - | - |
5″ | - | - | - | - | - | 176.6 | - | - |
6″ | - | - | - | - | - | 28.4 | - | - |
OCH3 | 60.1 | - | - | 56.7 | - | - | - | - |
CH3CO | - | 20.4, 170.1 | - | - | 20.4, 172.5 | - | - | - |
Solvent | DMSO-d6 | DMSO-d6 | * | DMSO-d6 | * | CD3OD | CDCl3 | DMSO-d6 |
References | [23] | [51] | [24] | [36] | [24] | [52] | [53] | [57] |
* The authors did not report the NMR solvent.