Table 25.
The 13C-NMR spectral data of compounds 53–64 except those which have no reported 13C-NMR data.
| C | 53 | 54 | 55 | 56 | 57 | 60 | 61 | 62 | 64 |
|---|---|---|---|---|---|---|---|---|---|
| 2 | 161.0 | 166.3 | 169.9 | 166.6 | 166.5 | 105.9 | 104.7 | 83.5 | 148.0 |
| 3 | 117.2 | 110.7 | 109.3 | 107.6 | 106.9 | 46.2 | 52.9 | 42.2 | 140.5 |
| 4 | 178.1 | 177.4 | 184.0 | 182.2 | 182.5 | 199.2 | 198.9 | 193.7 | 178.9 |
| 5 | 141.3 | 117.8 | 96.0 | 162.0 | 162.0 | 165.3 | 165.2 | 161.5 | 163.6 |
| 6 | 113.0 | 125.0 | 162.9 | 99.5 | 98.8 | 97.5 | 97.5 | 100.0 | 100.2 |
| 7 | 159.9 | 119.2 | 101.0 | 165.1 | 164.8 | 168.4 | 168.4 | 166.6 | 166.2 |
| 8 | 99.7 | 147.4 | 164.7 | 94.5 | 93.6 | 97.0 | 97.0 | 99.1 | 95.3 |
| 9 | 158.8 | 147.3 | 159.3 | 158.1 | 158.2 | 160.4 | 160.2 | 166.2 | 159.3 |
| 10 | 116.1 | 125.4 | 119.0 | 104.3 | 104.2 | 102.0 | 102.4 | 106.7 | 106.6 |
| 11 | 47.3 | 20.1 | 20.3 | 66.1 | 66.0 | 13.8 | 23.7 | 33.2 | - |
| 12 | 202.5 | - | - | - | - | - | 11.8 | 18.2 * | - |
| 13 | 29.8 | - | - | - | - | - | - | - | - |
| 14 | 22.3 | - | - | - | - | - | - | - | - |
| 1’ | 101.3 | 102.4 | 101.6 | 102.8 | 102.7 | 104.1 | 104.1 | 104.0 | 102.1 |
| 2’ | 73.1 | 74.8 | 74.7 | 73.9 | 73.6 | 75.0 | 75.0 | 74.6 | 72.0 |
| 3’ | 76.3 | 78.6 | 78.3 | 76.4 | 76.6 | 77.9 | 77.9 | 77.4 | 74.0 |
| 4’ | 69.5 | 71.2 | 71.4 | 67.7 | 70.1 | 71.0 | 71.0 | 71.2 | 71.5 |
| 5’ | 77.0 | 79.2 | 77.8 | 63.6 | 76.8 | 78.0 | 78.0 | 78.5 | 72.4 |
| 6’ | 60.9 | 62.4 | 62.4 | - | 61.3 | 62.5 | 62.5 | 62.5 | 62.5 |
| Solvent | DMSO-d6 | C5D5N | CD3OD | DMSO-d6 | CD3OD | CD3OD | CD3OD | CD3OD | CD3OD |
| References | [57] | [58] | [59] | [31] | [60] | [54] | [50] | [63] | [65] |
* Data interchangeable.