Table 26.
C | 66 | 67 | 68 | 69 | 70 | 71 | 72 |
---|---|---|---|---|---|---|---|
2 | 167.3 | 174.7 | 168.3 | 168.4 | 167.8 | 169.4 | 174.4 |
3 | 107.8 | 105.1 | 108.6 | 108.8 | 107.0 | 109.2 | 105.3 |
4 | 181.8 | 182.2 | 181.8 | 181.8 | 182.0 | 184.3 | 182.2 |
5 | 160.6 | 160.6 | 160.6 | 160.6 | 160.4 | 162.3 | 160.4 |
6 | 108.7 | 108.7 | 108.6 | 108.8 | 108.1 | 108.9 | 107.0 |
7 | 163.2 | 163.3 | 163.1 | 163.1 | 162.4 | 165.0 | 163.4 |
8 | 93.3 | 93.4 | 93.3 | 93.3 | 93.9 | 95.2 | 93.7 |
9 | 156.6 | 156.7 | 156.6 | 156.6 | 157.0 | 159.4 | 156.9 |
10 | 103.0 | 103.3 | 103.2 | 103.2 | 102.9 | 105.1 | 103.1 |
11 | 19.8 | 32.3 | 43.1 | 66.2 | 20.0 | 20.4 | 32.4 |
12 | - | 19.8 | 64.1 | 46.0 | - | - | 19.8 |
13 | - | 19.8 | 23.3 | 63.8 | - | - | 19.8 |
14 | - | - | - | 43.8 | - | - | - |
15 | - | - | - | 23.5 | - | - | - |
1′ | 73.0 | 73.0 | 72.9 | 72.9 | 70.8 | 75.6 | 70.7 |
2′ | 70.1 | 70.2 | 70.0 | 70.0 | 72.0 | 72.6 | 72.0 |
3′ | 78.9 | 78.9 | 78.8 | 78.8 | 76.7 | 80.1 | 76.6 |
4′ | 70.6 | 70.6 | 70.5 | 70.5 | 70.8 | 71.9 | 70.7 |
5′ | 81.4 | 81.6 | 81.4 | 81.4 | 82.0 | 80.2 | 81.8 |
6′ | 61.4 | 61.5 | 61.4 | 61.4 | 61.6 | 65.2 | 61.5 |
1″ | - | - | - | - | 119.9 | 121.6 | 119.9 |
2″ | - | - | - | - | 108.9 | 110.4 | 108.7 |
3″ | - | - | - | - | 145.4 | 146.6 | 145.4 |
4″ | - | - | - | - | 138.2 | 140.0 | 138.1 |
5″ | - | - | - | - | 145.4 | 146.6 | 145.4 |
6″ | - | - | - | - | 108.9 | 110.4 | 108.9 |
7″ | - | - | - | - | 164.8 | 168.6 | 164.7 |
Solvent | DMSO-d6 | DMSO-d6 | DMSO-d6 | DMSO-d6 | DMSO-d6 | CD3OD | DMSO-d6 |
References | [69] | [69] | [72] | [72] | [71] | [73] | [69] |