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. 2021 Dec 16;26(24):7646. doi: 10.3390/molecules26247646

Table 28.

The 13C-NMR spectral data of compounds 80–89.

C 80 81 82 83 84 85 86 87 88 89
2 167.0 169.3 174.4 173.0 168.2 167.6 167.2 174.8 167.7 174.5
3 107.4 108.7 105.0 106.2 108.3 107.8 107.5 105.4 108.0 105.6
4 181.9 184.3 182.2 181.9 181.9 182.2 181.9 182.4 182.2 182.4
5 160.4 149.4 160.4 160.4 160.3 160.8 160.5 160.7 161.0 161.0
6 98.4 94.5 98.5 98.7 98.3 97.6 98.3 97.8 98.0 97.9
7 162.5 162.8 162.8 164.2 162.7 162.2 162.6 162.3 162.4 162.6
8 104.3 105.2 104.1 104.7 108.4 103.9 104.0 102.8 103.9 102.1
9 156.1 164.6 156.5 156.6 158.9 157.1 156.3 157.2 157.1 157.2
10 103.5 106.3 102.0 103.3 103.8 102.8 103.5 104.0 102.0 104.0
11 19.6 20.3 32.7 39.1 42.1 11.0 19.7 33.1 20.1 33.1
12 - - 20.0 27.0 66.5 - - 19.8 - 20.3
13 - - 19.5 11.4 45.8 - - 20.3 - 20.1
14 - - - 17.4 64.1 - - - - -
15 - - - - 23.6 - - - - -
1′ 73.1 74.9 73.1 73.3 73.2 70.6 73.3 70.7 70.7 70.8
2′ 71.0 72.8 71.2 71.2 70.3 72.5 70.0 72.5 70.1 70.2
3′ 78.5 80.0 78.5 78.7 78.6 76.1 78.1 76.0 77.0 77.0
4′ 70.3 71.7 70.8 70.9 71.0 70.8 70.7 71.2 68.5 68.9
5′ 81.1 82.4 81.5 81.5 81.4 81.7 78.3 82.0 81.5 81.9
6′ 61.3 62.9 61.8 61.7 61.5 61.5 63.8 61.8 61.0 61.3
1″ - - - - - 119.7 119.4 119.6 119.6 119.6
2″ , 6″ - - - - - 108.8 108.5 108.7 108.9 108.9
3″ , 5″ - - - - - 145.5 145.5 145.4 145.6 145.5
4″ - - - - - 138.8 138.3 138.3 138.7 138.7
7″ - - - - - 165.0 165.8 165.0 165.5 165.4
1‴ - - - - - - - - 118.7 118.7
2‴ , 6‴ - - - - - - - - 108.7 108.7
3‴ , 5‴ - - - - - - - - 145.5 145.4
4‴ - - - - - - - - 138.5 138.6
7‴ - - - - - - - - 164.8 164.8
OCH3 - 56.8 - - - - - - - -
Solvent DMSO-d6 CD3OD DMSO-d6 DMSO-d6 DMSO-d6 DMSO-d6 DMSO-d6 DMSO-d6 DMSO-d6 DMSO-d6
References [86] [87] [158] [158] [72] [71] [91] [69] [71] [71]