Table 30.
C | 103 | 104 | 106 | 107 | 108 | 109 | 110 |
---|---|---|---|---|---|---|---|
2 | 165.0 | 165.0 | 167.4 | 167.2 | 167.4 | 167.1 | 167.2 |
3 | 111.3 | 111.3 | 112.5 | 112.6 | 112.6 | 111.9 | 111.9 |
4 | 178.6 | 178.8 | 182.3 | 182.2 | 182.2 | 181.9 | 182.0 |
5 | 141.7 | 141.8 | 144.6 | 144.8 | 144.6 | 144.3 | 144.3 |
6 | 111.0 | 111.3 | 112.7 | 112.6 | 112.5 | 112.3 | 112.4 |
7 | 159.5 | 159.8 | 162.1 | 162.0 | 162.0 | 161.6 | 161.6 |
8 | 110.6 | 110.7 | 111.8 | 111.4 | 111.8 | 111.6 | 111.3 |
9 | 157.4 | 157.5 | 159.8 | 159.6 | 159.6 | 159.3 | 159.1 |
10 | 115.8 | 115.8 | 117.2 | 117.2 | 117.2 | 116.9 | 116.9 |
11 | 43.1 | 43.3 | 44.6 | 44.9 | 44.6 | 44.5 | 44.3 |
12 | 64.4 | 63.9 | 65.9 | 66.3 | 66.0 | 66.6 | 66.5 |
13 | 23.3 | 23.7 | 23.6 | 23.7 | 23.6 | 23.5 | 23.6 |
14 | 22.8 | 22.9 | 23.7 | 23.7 | 23.6 | 23.5 | 23.3 |
15 | 56.5 | 56.5 | 57.0 | 57.1 | 57.0 | 56.9 | 57.0 |
1′ | 70.6 | 70.6 | 72.8 | 72.8 | 72.8 | 71.9 | 71.8 |
2′ | 72.6 | 72.3 | 73.4 | 73.7 | 73.9 | 74.0 | 73.7 |
3′ | 75.7 | 75.9 | 77.7 | 77.7 | 77.9 | 77.6 | 77.4 |
4′ | 70.4 | 70.9 | 72.4 | 72.4 | 72.3 | 72.4 | 72.4 |
5′ | 81.8 | 82.0 | 83.0 | 80.1 | 82.9 | 82.7 | 82.4 |
6′ | 61.5 | 61.6 | 63.1 | 64.4 | 63.1 | 62.9 | 62.7 |
1″ | 133.9 | 125.0 | 127.0 | 127.0 | 128.2 | 135.3 | 126.7 |
2″ | 128.9 | 130.3 | 133.2 | 131.1 | 130.9 | 128.9 | 130.9 |
3″ | 128.2 | 115.8 | 115.7 | 116.9 | 115.4 | 129.7 | 116.6 |
4″ | 130.4 | 159.6 | 160.0 | 161.3 | 163.2 | 131.3 | 160.7 |
5″ | 128.2 | 115.8 | 115.7 | 116.9 | 115.4 | 129.7 | 116.6 |
6″ | 128.9 | 130.3 | 133.2 | 131.1 | 130.9 | 128.9 | 130.9 |
7″ | 144.1 | 144.4 | 145.0 | 146.6 | 146.1 | 146.1 | 146.4 |
8″ | 117.8 | 114.0 | 115.7 | 114.6 | 115.6 | 118.1 | 114.2 |
9″ | 165.0 | 165.4 | 167.6 | 168.0 | 167.8 | 167.2 | 167.8 |
OCH3 | - | - | - | - | 55.9 | - | - |
COCH3 | - | - | - | 173.0, 20.9 | - | - | - |
Solvent | DMSO-d6 | DMSO-d6 | CD3OD | CD3OD | CD3OD | CD3OD | CD3OD |
References | [99] | [159] | [80] | [100] | [100] | [82] | [82] |