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. 2021 Dec 16;26(24):7646. doi: 10.3390/molecules26247646

Table 30.

The 13C-NMR spectral data of compounds 103110 except which has no reported 13C-NMR data.

C 103 104 106 107 108 109 110
2 165.0 165.0 167.4 167.2 167.4 167.1 167.2
3 111.3 111.3 112.5 112.6 112.6 111.9 111.9
4 178.6 178.8 182.3 182.2 182.2 181.9 182.0
5 141.7 141.8 144.6 144.8 144.6 144.3 144.3
6 111.0 111.3 112.7 112.6 112.5 112.3 112.4
7 159.5 159.8 162.1 162.0 162.0 161.6 161.6
8 110.6 110.7 111.8 111.4 111.8 111.6 111.3
9 157.4 157.5 159.8 159.6 159.6 159.3 159.1
10 115.8 115.8 117.2 117.2 117.2 116.9 116.9
11 43.1 43.3 44.6 44.9 44.6 44.5 44.3
12 64.4 63.9 65.9 66.3 66.0 66.6 66.5
13 23.3 23.7 23.6 23.7 23.6 23.5 23.6
14 22.8 22.9 23.7 23.7 23.6 23.5 23.3
15 56.5 56.5 57.0 57.1 57.0 56.9 57.0
1′ 70.6 70.6 72.8 72.8 72.8 71.9 71.8
2′ 72.6 72.3 73.4 73.7 73.9 74.0 73.7
3′ 75.7 75.9 77.7 77.7 77.9 77.6 77.4
4′ 70.4 70.9 72.4 72.4 72.3 72.4 72.4
5′ 81.8 82.0 83.0 80.1 82.9 82.7 82.4
6′ 61.5 61.6 63.1 64.4 63.1 62.9 62.7
1″ 133.9 125.0 127.0 127.0 128.2 135.3 126.7
2″ 128.9 130.3 133.2 131.1 130.9 128.9 130.9
3″ 128.2 115.8 115.7 116.9 115.4 129.7 116.6
4″ 130.4 159.6 160.0 161.3 163.2 131.3 160.7
5″ 128.2 115.8 115.7 116.9 115.4 129.7 116.6
6″ 128.9 130.3 133.2 131.1 130.9 128.9 130.9
7″ 144.1 144.4 145.0 146.6 146.1 146.1 146.4
8″ 117.8 114.0 115.7 114.6 115.6 118.1 114.2
9″ 165.0 165.4 167.6 168.0 167.8 167.2 167.8
OCH3 - - - - 55.9 - -
COCH3 - - - 173.0, 20.9 - - -
Solvent DMSO-d6 DMSO-d6 CD3OD CD3OD CD3OD CD3OD CD3OD
References [99] [159] [80] [100] [100] [82] [82]