Table 32.
C | 123 | 124 | 126 | 127 | 128 | 129 |
---|---|---|---|---|---|---|
2 | 167.7 | 168.3 | 171.3 | 170.7 | 167.7 | 169.9 |
3 | 108.0 | 108.5 | 105.6 | 105.5 | 108.3 | 108.4 |
4 | 182.2 | 182.4 | 184.3 | 183.0 | 182.7 | 182.4 |
5 | 158.8 | 157.8 | 160.2 | 158.1 | 159.5 | 159.6 |
6 | 110.4 | 111.1 | 112.5 | 112.8 | 107.4 | 105.2 |
7 | 162.3 | 163.1 | 163.8 | 161.0 | 162.9 | 163.1 |
8 | 93.2 | 90.5 | 94.4 | 93.0 | 92.8 | 92.9 |
9 | 156.1 | 156.6 | 157.8 | 156.1 | 156.7 | 156.4 |
10 | 103.3 | 104.4 | 106.8 | 105.6 | 103.4 | 103.8 |
11 | 19.9 | 19.9 | 61.6 | 60.0 | 18.8 | 60.0 |
OCH3 | - | 56.5 | - | - | - | - |
1′ | 20.5 | 20.5 | 22.1 | 20.5 | 26.4 | 26.4 |
2′ | 126.9 | 126.4 | 128.7 | 124.6 | 79.9 | 79.8 |
3′ | 131.8 | 132.3 | 132.9 | 134.1 | 143.7 | 143.7 |
4′ | 66.1 | 66.1 | 68.4 | 61.0 | 114.2 | 114.2 |
5′ | 21.2 | 21.3 | 21.9 | 20.0 | 15.2 | 15.2 |
1″ | 101.5 | 101.6 | 102.7 | 100.1 | 99.4 | 99.4 |
2″ | 73.6 | 73.6 | 75.3 | 73.2 | 73.6 | 73.6 |
3″ | 76.9 | 77.0 | 78.3 | 76.7 | 76.3 | 76.3 |
4″ | 70.2 | 70.2 | 71.8 | 67.7 | 70.2 | 70.2 |
5″ | 77.0 | 77.0 | 77.9 | 77.0 | 76.7 | 76.7 |
6″ | 61.1 | 61.1 | 62.9 | 60.1 | 61.2 | 61.2 |
Solvent | DMSO-d6 | DMSO-d6 | CD3OD | CD3OD | CD3OD | CD3OD |
References | [104] | [104] | [106] | [60] | [60] | [60] |