Table 33.
C | 130 | 131 | 132 | 133 | 134 | 135 | 136 | 137 | 138 | 139 |
---|---|---|---|---|---|---|---|---|---|---|
2 | 170.7 | 167.6 | 170.7 | 168.3 | 171.4 | 168.9 | 165.0 | 171.0 | 171.5 | 171.8 |
3 | 105.5 | 107.4 | 104.9 | 108.1 | 105.5 | 113.9 | * | 110.4 | 110.7 | 110.7 |
4 | 183.0 | 181.8 | 181.9 | 182.5 | 182.5 | 176.6 | * | 179.3 | 180.4 | 180.6 |
5 | 158.8 | 158.8 | 158.9 | 159.5 | 159.5 | 132.6 | * | 106.6 | 119.2 | 126.2 |
6 | 111.4 | 97.6 | 97.8 | 98.3 | 98.4 | 111.4 | 99.3 | 150.7 | 126.2 | 126.6 |
7 | 162.1 | 159.9 | 160.1 | 160.6 | 160.8 | 158.2 | 162.9 | 153.1 | 122.1 | 135.6 |
8 | 93.3 | 107.5 | 107.4 | 108.1 | 108.2 | 103.6 | 94.8 | 106.9 | 147.8 | 119.3 |
9 | 156.3 | 153.8 | 153.5 | 154.4 | 154.1 | 163.4 | * | 149.8 | 149.0 | 158.0 |
10 | 105.7 | 104.3 | 104.8 | 105.0 | 105.4 | 112.7 | * | 116.2 | 125.0 | 124.3 |
11 | 60.0 | 19.5 | 59.3 | 20.2 | 59.5 | 127.9 | 121.6 | 102.2 | 141.4 | 136.2 |
1′ | 28.2 | 20.3 | 20.3 | 21.0 | 20.9 | 131.9 | 128.5 | 74.3 | 129.5 | 114.0 |
2′ | 74.6 | 120.5 | 120.4 | 121.1 | 121.0 | 115.7 | 115.7 | 78.1 | 129.6 | 150.7 |
3′ | 147.9 | 134.9 | 134.9 | 135.6 | 135.7 | 157.1 | 161.5 | 71.5 | 127.4 | 146.4 |
4′ | 109.5 | 65.9 | 65.8 | 66.5 | 66.5 | 115.7 | 115.7 | 78.0 | 129.6 | 118.1 |
5′ | 16.6 | 13.1 | 13.1 | 13.8 | 13.7 | 131.9 | 128.5 | 62.8 | 129.5 | 122.0 |
6′ | - | - | - | - | - | 39.3 | 39.1 | - | 33.8 | 33.6 |
7′ | - | - | - | - | - | 86.3 | 37.5 | - | 37.0 | 37.1 |
8′ | - | - | - | - | - | 127.9 | 121.6 | 102.2 | 141.4 | 136.2 |
1″ | 101.2 | 100.1 | 100.1 | 100.7 | 100.7 | 101.8 | 100.3 | 131.5 | 103.0 | 102.9 |
2″ | 73.6 | 72.9 | 72.9 | 73.5 | 73.5 | 74.6 | * | 133.0 | 75.0 | 74.9 |
3″ | 76.5 | 76.7 | 76.7 | 76.7 | 76.7 | 78.4 | * | 116.3 | 78.2 | 77.8 |
4″ | 69.8 | 69.2 | 69.2 | 69.8 | 69.8 | 71.2 | * | 164.1 | 71.3 | 71.3 |
5″ | 77.1 | 76.1 | 76.1 | 77.3 | 77.3 | 78.2 | * | 116.3 | 78.2 | 78.1 |
6″ | 61.1 | 60.2 | 60.2 | 60.8 | 60.8 | 62.5 | * | 120.9 | 62.5 | 62.4 |
7″ | - | - | - | - | - | - | - | 33.9 | - | - |
8″ | - | - | - | - | - | - | - | 37.1 | - | - |
OCH3 | - | - | - | - | - | - | - | 6-OCH3 56.3 4″-OCH3 55.1 |
- | 56.6 |
Solvent | CD3OD | DMSO-d6 | DMSO-d6 | DMSO-d6 | DMSO-d6 | CD3OD | DMSO-d6 | DMSO-d6 | CD3OD | CD3OD |
References | [60] | [108] | [108] | [109] | [109] | [110] | [111] | [112] | [113] | [114] |
* The authors missed assigning these positions.