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. 2021 Dec 16;26(24):7646. doi: 10.3390/molecules26247646

Table 33.

The 13C-NMR spectral data of compounds 130139.

C 130 131 132 133 134 135 136 137 138 139
2 170.7 167.6 170.7 168.3 171.4 168.9 165.0 171.0 171.5 171.8
3 105.5 107.4 104.9 108.1 105.5 113.9 * 110.4 110.7 110.7
4 183.0 181.8 181.9 182.5 182.5 176.6 * 179.3 180.4 180.6
5 158.8 158.8 158.9 159.5 159.5 132.6 * 106.6 119.2 126.2
6 111.4 97.6 97.8 98.3 98.4 111.4 99.3 150.7 126.2 126.6
7 162.1 159.9 160.1 160.6 160.8 158.2 162.9 153.1 122.1 135.6
8 93.3 107.5 107.4 108.1 108.2 103.6 94.8 106.9 147.8 119.3
9 156.3 153.8 153.5 154.4 154.1 163.4 * 149.8 149.0 158.0
10 105.7 104.3 104.8 105.0 105.4 112.7 * 116.2 125.0 124.3
11 60.0 19.5 59.3 20.2 59.5 127.9 121.6 102.2 141.4 136.2
1′ 28.2 20.3 20.3 21.0 20.9 131.9 128.5 74.3 129.5 114.0
2′ 74.6 120.5 120.4 121.1 121.0 115.7 115.7 78.1 129.6 150.7
3′ 147.9 134.9 134.9 135.6 135.7 157.1 161.5 71.5 127.4 146.4
4′ 109.5 65.9 65.8 66.5 66.5 115.7 115.7 78.0 129.6 118.1
5′ 16.6 13.1 13.1 13.8 13.7 131.9 128.5 62.8 129.5 122.0
6′ - - - - - 39.3 39.1 - 33.8 33.6
7′ - - - - - 86.3 37.5 - 37.0 37.1
8′ - - - - - 127.9 121.6 102.2 141.4 136.2
1″ 101.2 100.1 100.1 100.7 100.7 101.8 100.3 131.5 103.0 102.9
2″ 73.6 72.9 72.9 73.5 73.5 74.6 * 133.0 75.0 74.9
3″ 76.5 76.7 76.7 76.7 76.7 78.4 * 116.3 78.2 77.8
4″ 69.8 69.2 69.2 69.8 69.8 71.2 * 164.1 71.3 71.3
5″ 77.1 76.1 76.1 77.3 77.3 78.2 * 116.3 78.2 78.1
6″ 61.1 60.2 60.2 60.8 60.8 62.5 * 120.9 62.5 62.4
7″ - - - - - - - 33.9 - -
8″ - - - - - - - 37.1 - -
OCH3 - - - - - - - 6-OCH3 56.3
4″-OCH3 55.1
- 56.6
Solvent CD3OD DMSO-d6 DMSO-d6 DMSO-d6 DMSO-d6 CD3OD DMSO-d6 DMSO-d6 CD3OD CD3OD
References [60] [108] [108] [109] [109] [110] [111] [112] [113] [114]

* The authors missed assigning these positions.