Table 34.
The 13C-NMR spectral data of compounds 140–148.
| C | 140 | 141 | 142 | 143 | 144 | 145 | 146 | 147 | 148 |
|---|---|---|---|---|---|---|---|---|---|
| 2 | 147.2 | 146.9 | 147.3 | 89.9 | 89.0 | 92.9 | 92.1 | 92.3 | 88.2 |
| 3 | 106.1 | 105.0 | 104.9 | 24.3 | 28.3 | 28.1 | 27.9 | 28.0 | 30.1 |
| 4 | 153.7 | 160.5 | 159.2 | 165.5 | 164.5 | 160.3 | 165.3 | 156.3 | 158.5 |
| 5 | 177.2 | 185.9 | 184.7 | 176.9 | 176.4 | 184.7 | 176.6 | 176.6 | 182.9 |
| 6 | 109.7 | 107.8 | 107.2 | 111.9 | 109.8 | 109.5 | 110.9 | 111.4 | 107.2 |
| 7 | 163.7 | 169.0 | 168.7 | 163.3 | 164.0 | 169.7 | 162.7 | 162.6 | 166.7 |
| 9 | 95.8 | 92.0 | 92.0 | 94.8 | 95.2 | 90.4 | 94.0 | 94.2 | 88.8 |
| 10 | 157.8 | 156.1 | 154.5 | 159.9 | 160.1 | 168.3 | 159.7 | 165.4 | 166.6 |
| 11 | 117.0 | 114.3 | 113.4 | 118.7 | 117.2 | 111.3 | 118.1 | 118.5 | 108.7 |
| 12 | 152.8 | 106.9 | 106.3 | 112.3 | 111.4 | 106.6 | 112.5 | 112.8 | 102.9 |
| 13 | 155.6 | 155.7 | 155.2 | 156.4 | 157.7 | 157.9 | 156.1 | 159.9 | 158.6 |
| 14 | 65.7 | 67.8 | 66.3 | 21.4 | 20.7 | 20.8 | 66.4 | 66.8 | 66.1 |
| 4-OCH3 | 61.9 | - | - | - | * | - | 60.8 | 61.0 | - |
| 1′ | 103.0 | 104.4 | 104.4 | 77.3 | 74.3 | 79.7 | 70.8 | 70.8 | 143.7 |
| 2′ | 74.0 | 75.0 | 74.2 | 23.4 | 24.1 | 24.3 | 26.0 | 26.2 | 115.5 |
| 3′ | 77.2 | 77.9 | 77.6 | 22.3 | 23.5 | 23.0 | 25.6 | 25.8 | 15.7 |
| 4′ | 70.6 | 71.6 | 70.9 | - | - | - | - | - | - |
| 5′ | 77.1 | 78.0 | 76.7 | - | - | - | - | - | - |
| 6′ | 61.7 | 68.7 | 69.5 | - | - | - | - | - | - |
| 1″ | - | 111.1 | 103.3 | 98.9 | 100.1 | 99.5 | 104.0 | 104.4 | 102.8 |
| 2″ | - | 77.2 | 74.4 | 75.1 | 74.6 | 75.6 | 74.8 | 75.0 | 73.7 |
| 3″ | - | 80.6 | 77.4 | 78.8 | 78.6 | 78.5 | 78.4 | 78.3 | 76.7 |
| 4″ | - | 74.9 | 70.9 | 71.3 | 71.4 | 72.0 | 71.4 | 71.3 | 70.3 |
| 5″ | - | 65.5 | 77.7 | 77.1 | 78.2 | 76.8 | 78.1 | 75.7 | 76.9 |
| 6″ | - | - | 61.9 | 62.4 | 63.1 | 68.5 | 62.6 | 64.5 | 61.4 |
| 1‴ | - | - | - | - | - | 111.2 | - | 126.5 | - |
| 2‴ | - | - | - | - | - | 78.6 | - | 111.4 | - |
| 3‴ | - | - | - | - | - | 81.0 | - | 149.0 | - |
| 4‴ | - | - | - | - | - | 75.6 | - | 151.2 | - |
| 5‴ | - | - | - | - | - | 66.2 | - | 116.8 | - |
| 6‴ | - | - | - | - | - | - | - | 123.9 | - |
| 7‴ | - | - | - | - | - | - | - | 145.9 | - |
| 8‴ | - | - | - | - | - | - | - | 115.1 | - |
| 9‴ | - | - | - | - | - | - | - | 167.8 | - |
| 3‴-OCH3 | - | - | - | - | - | - | - | 55.9 | - |
| Solvent | DMSO-d6, C6D6 | CD3OD | DMSO-d6 | CDCl3, CD3OD | CDCl3, CD3OD | CD3OD | C5D5N | C5D5N | CD3OD |
| References | [117] | [118] | [109] | [122] | [122] | [119] | [121] | [132] | [60] |
* The authors missed assigning this position.