Skip to main content
. 2021 Dec 16;26(24):7646. doi: 10.3390/molecules26247646

Table 36.

The 13C-NMR spectral data of compounds 157–165.

C 157 158 159 160 161 162 163 164 165
Chromone
moiety
2′ 92.4 92.2 92.2 92.2 92.2 92.2 92.2 92.2 92.2
3′ 27.9 27.8 27.8 27.8 27.8 27.8 27.8 27.8 27.8
4′ 156.3 156.2 156.2 156.2 156.2 156.2 156.2 156.2 156.1
5′ 176.2 176.2 176.2 176.2 176.2 176.2 176.3 176.3 176.3
6′ 111.5 110.9 111.1 110.9 110.9 110.8 111.1 111.2 111.1
7′ 162.1 162.5 162.4 162.4 162.7 162.5 162.6 162.6 162.5
9′ 94.1 94.0 94.0 94.0 94.1 94.0 94.0 94.1 94.0
10′ 165.4 165.2 165.2 165.2 165.2 165.2 165.2 165.2 165.2
11′ 118.5 118.4 118.4 118.4 118.4 118.4 118.4 118.4 118.4
12′ 112.9 112.8 112.8 112.5 112.8 112.8 112.8 112.8 112.7
13′ 159.9 159.8 159.8 159.7 159.8 159.7 159.8 159.9 159.8
14′ 66.3 66.3 66.5 66.2 66.4 66.2 66.5 66.3 66.5
4-OCH3 60.9 60.9 60.9 60.8 60.9 60.9 60.9 60.9 60.8
1″ 70.6 70.6 70.6 70.6 70.6 70.6 70.6 70.7 70.6
2″ 26.0 26.1 26.1 26.1 26.1 26.1 26.1 26.2 26.1
3″ 25.6 25.7 25.7 25.6 25.7 25.7 25.6 25.6 25.7
Glu-1 101.7 104.1 104.2 104.1 104.1 104.0 104.2 103.9 104.3
Glu-2 74.5 74.9 74.8 74.8 74.9 74.9 74.9 74.8 74.9
Glu-3 79.1 78.3 78.1 78.4 78.4 78.4 78.4 78.2 78.1
Glu-4 69.3 71.2 71.4 71.4 71.5 71.3 71.5 72.0 71.9
Glu-5 78.4 76.9 75.4 77.1 77.1 76.7 77.0 76.8 76.7
Glu-6 62.4 63.5 64.2 62.7 62.7 62.8 62.6 62.9 62.7
Triterpene
moiety
1 31.8 31.9 31.9 32.3 30.3 32.0 27.4 31.9 31.9
2 29.8 29.8 30.0 30.0 29.5 30.0 29.8 29.6 29.8
3 87.8 88.0 88.3 88.4 88.1 88.3 88.3 88.0 88.0
4 41.1 40.3 41.2 41.2 41.2 41.2 40.7 41.1 41.1
5 47.1 47.0 47.4 47.4 42.6 47.4 43.8 47.0 46.9
6 20.5 20.4 20.8 20.9 21.7 20.8 22.0 20.4 20.3
7 25.6 25.8 25.9 26.4 113.2 26.3 114.0 25.8 25.7
8 46.0 45.9 47.1 49.0 149.1 47.3 148.6 45.8 46.4
9 19.8 19.9 19.2 19.9 21.1 19.5 27.6 20.0 20.5
10 26.5 26.6 26.6 26.5 28.2 26.4 29.1 26.6 27.0
11 36.7 36.6 26.3 26.4 25.4 26.1 63.2 36.7 36.4
12 77.2 76.8 31.4 34.0 33.9 33.3 48.3 77.2 76.9
13 48.8 48.7 42.2 41.8 41.2 46.6 45.4 48.7 48.8
14 47.2 47.4 45.2 46.5 49.8 45.1 48.1 47.8 47.8
15 43.4 43.4 50.8 82.5 80.4 42.8 45.2 43.8 45.6
16 70.7 72.8 218.6 103.0 103.3 72.5 114.5 71.1 74.6
17 55.7 55.6 60.4 60.5 60.3 51.4 61.0 56.8 52.4
18 13.5 13.5 18.8 20.3 22.5 20.5 20.7 13.5 12.9
19 29.9 30.7 30.0 30.7 28.2 30.1 18.7 29.8 30.0
20 26.9 25.4 29.1 27.6 27.5 34.2 23.7 26.0 24.6
21 21.1 20.8 19.9 21.4 21.6 17.3 19.6 21.1 25.7
22 41.5 38.6 40.3 33.6 33.6 86.2 37.8 41.9 106.0
23 104.2 102.9 173.4 74.2 74.4 109.6 71.7 101.9 152.9
24 83.1 212.4 - 80.5 80.4 77.3 88.5 77.7 75.9
25 79.1 35.0 - 76.4 76.5 83.5 76.4 81.3 78.2
26 19.4 19.2 - 21.6 21.6 27.3 23.2 23.7 22.3
27 29.8 19.7 - 24.1 24.1 24.5 20.2 24.9 23.1
28 19.4 19.4 19.6 11.8 18.2 19.4 27.4 19.5 20.7
29 25.6 25.6 25.6 25.5 25.6 25.6 25.8 25.6 25.6
30 15.2 15.2 15.2 15.5 14.2 15.3 14.5 15.2 15.2
Xyl-1 107.4 107.5 107.5 107.4 107.4 107.4 107.4 107.5 107.5
Xyl-2 75.5 75.5 75.5 75.5 75.5 75.5 75.5 75.5 75.5
Xyl-3 78.5 78.6 78.5 78.5 78.5 78.5 78.5 78.5 78.5
Xyl-4 71.1 71.0 71.1 71.1 71.2 71.1 71.1 71.2 71.1
Xyl-5 67.0 67.0 67.1 67.0 67.0 67.0 67.0 67.0 67.0
COCH3 170.4
21.5		 170.4
21.5		 - 171.0
21.1		 171.0
21.1		 - - 170.5
21.6		 170.6
21.1
Solvent C5D5N C5D5N C5D5N C5D5N C5D5N C5D5N C5D5N C5D5N C5D5N
References [130] [130] [130] [130] [130] [130] [130] [136] [136]