Table 40.
The 13C-NMR spectral data of compounds 184–192.
| C | 184 | 185 | 186 | 187 | 188 | 189 | 190 | 191 | 192 |
|---|---|---|---|---|---|---|---|---|---|
| 2 | 167.5 | 167.4 | 167.0 | 167.0 | 165.7 | 165.7 | 167.5 | 169.3 | 169.3 |
| 3 | 111.1 | 110.9 | 110.9 | 110.8 | 111.3 | 111.3 | 111.1 | 109.1 | 109.1 |
| 4 | 180.2 | 180.0 | 179.4 | 179.4 | 178.5 | 178.6 | 180.2 | 182.4 | 182.5 |
| 4a | 126.6 | 126.4 | 126.5 | 126.4 | 126.3 | 126.3 | 126.6 | 113.3 | 113.3 |
| 5 | 149.2 | 149.1 | 149.4 | 149.2 | 148.2 | 148.2 | 149.3 | 166.7 | 166.7 |
| 6 | 122.5 | 122.4 | 122.9 | 122.8 | 124.1 | 124.0 | 122.5 | 110.7 | 110.7 |
| 6a | 137.2 | 137.1 | 137.0 | 136.9 | 136.9 | 136.9 | 137.2 | 139.8 | 139.9 |
| 7 | 181.2 | 181.0 | 181.2 | 181.2 | 181.5 | 181.4 | 181.2 | 180.8 | 180.8 |
| 7a | 130.3 | 130.2 | 130.4 | 130.3 | 130.5 | 130.5 | 130.5 | 130.6 | 130.4 |
| 8 | 119.8 | 119.7 | 119.7 | 119.7 | 119.5 | 119.5 | 119.8 | 119.4 | 119.5 |
| 9 | 133.6 | 133.7 | 133.4 | 133.6 | 133.3 | 133.5 | 133.7 | 132.4 | 132.8 |
| 10 | 141.3 | 141.1 | 141.0 | 140.9 | 141.0 | 140.9 | 140.7 | 140.2 | 140.9 |
| 11 | 159.1 | 159.2 | 159.3 | 158.9 | 159.3 | 159.3 | 159.4 | 159.1 | 159.1 |
| 11a | 115.8 | 115.6 | 115.9 | 115.7 | 115.9 | 115.9 | 115.9 | 115.6 | 115.4 |
| 12 | 186.9 | 186.9 | 187.1 | 186.9 | 187.5 | 187.4 | 186.9 | 186.2 | 186.3 |
| 12a | 121.8 | 121.6 | 121.6 | 121.6 | 120.8 | 120.8 | 121.8 | 112.3 | 112.4 |
| 12b | 156.8 | 156.7 | 156.6 | 156.5 | 156.1 | 156.1 | 156.8 | 156.6 | 156.6 |
| 13 | 80.9 | 80.0 | 79.0 | 78.9 | 48.3 | 48.2 | 80.9 | - | - |
| 14 | 59.8 | 59.7 | 59.8 | 59.7 | 59.8 | 59.7 | 59.8 | 60.0 | 60.0 |
| 15 | 19.7 | 19.6 | 19.8 | 19.7 | 20.0 | 19.9 | 19.6 | 19.6 | 19.7 |
| 16 | 62.7 | 62.5 | 62.5 | 62.5 | 62.5 | 62.5 | 62.7 | 62.7 | 62.7 |
| 17 | 13.4 | 13.3 | 13.4 | 13.3 | 13.5 | 13.4 | 13.3 | 13.2 | 13.2 |
| 18 | 170.5 | 170.4 | 170.9 | 170.9 | 170.4 | 170.4 | 170.5 | - | - |
| 19 | 52.6 | 52.5 | 52.4 | 52.3 | 52.3 | 52.3 | 52.6 | - | - |
| 2′ | 73.8 | 73.8 | 74.9 | 74.9 | 74.3 | 74.2 | 73.8 | - | - |
| 3′ | 68.9 | 68.9 | 68.5 | 68.2 | 68.8 | 68.8 | 69.0 | - | - |
| 4′ | 80.2 | 80.1 | 74.8 | 74.9 | 81.5 | 81.4 | 80.2 | - | - |
| 5′ | 67.9 | 67.9 | 26.1 | 26.0 | 68.0 | 67.9 | 68.0 | - | - |
| 6′ | 73.7 | 73.6 | 70.3 | 70.2 | 73.9 | 74.0 | 73.7 | - | - |
| 7′ | 14.1 | 14.0 | 14.7 | 14.7 | 14.7 | 14.6 | 14.0 | - | - |
| 4′-OCH3 | 57.9 | 57.8 | 55.6 | 55.5 | 57.1 | 57.1 | 58.0 | - | - |
| 2″ | 70.3 | 70.7 | 70.2 | 70.8 | 70.3 | 70.8 | 70.0 | 70.0 | 70.7 |
| 3″ | 77.7 | 82.6 | 77.8 | 82.7 | 77.8 | 82.8 | 76.0 | 77.3 | 82.8 |
| 4″ | 54.9 | 58.1 | 55.1 | 58.1 | 54.9 | 58.1 | 51.7 | 56.1 | 58.1 |
| 5″ | 40.3 | 44.7 | 40.4 | 44.7 | 40.4 | 44.8 | 44.9 | 38.5 | 44.8 |
| 6″ | 62.1 | 62.2 | 62.3 | 62.2 | 62.2 | 62.3 | 62.3 | 63.6 | 62.3 |
| 7″ | 14.7 | 13.5 | 14.8 | 13.5 | 14.7 | 13.6 | 14.1 | 15.4 | 13.6 |
| 8″ | 24.1 | 14.0 | 23.8 | 13.9 | 24.2 | 14.1 | 32.6 | 22.6 | 14.0 |
| 4″-N(CH3)n | 27.9 | 40.3 | 27.8 | 40.3 | 28.1 | 40.4 | - | 27.2 | 40.3 |
| 1‴ | 93.4 | 94.4 | 93.7 | 94.5 | 93.4 | 94.5 | 93.3 | 94.5 | 94.5 |
| 2‴ | 30.8 | 31.1 | 30.9 | 31.1 | 30.9 | 31.1 | 30.8 | 31.1 | 31.1 |
| 3‴ | 74.8 | 74.9 | 74.8 | 74.9 | 74.9 | 75.0 | 74.8 | 75.0 | 75.0 |
| 4‴ | 72.1 | 72.1 | 72.1 | 72.0 | 72.2 | 72.2 | 72.2 | 71.5 | 72.2 |
| 5‴ | 65.4 | 65.0 | 65.7 | 65.0 | 65.4 | 65.1 | 65.4 | 66.6 | 65.0 |
| 6‴ | 17.7 | 17.6 | 17.7 | 17.6 | 17.8 | 17.7 | 17.8 | 17.5 | 17.7 |
| 3‴-OCH3 | 55.9 | 56.1 | 56.1 | 56.1 | 55.9 | 56.2 | 56.0 | 56.4 | 56.1 |
| Solvent | CDCl3 | CDCl3 | CDCl3 | CDCl3 | CDCl3 | CDCl3 | CDCl3 | CDCl3 | CDCl3 |
| References | [149] | [149] | [149] | [149] | [137] | [137] | [137] | [137] | [137] |