Table 1.
On-line mass fingerprinting of crude venom extract from Campsomeriella annulata annulata by LC-ESI-MS.
| Fr. No. | Retention Time (min) | [M + H]+ m/z |
|---|---|---|
| 1 | 0.8–1.5 | 90.054, 112.086, 116.069, 118.085, 120.064, 146.164, 147.075, 148.059, 154.085, 156.076, 175.118, 203.222, 258.108, 752.482 |
| 2 | 1.5–2.0 | 132.101, 138.090, 150.057, 182.080, 245.075, 253.116, 268.102, 284.097, 324.126, 348.067, 664.111 |
| 3 | 2.0–3.0 | 166.085, 269.086, 732.288, 873.461, 911.428, 916.637, 952.596, 1006.514, 1050.563, 1377.700, 1629.831 |
| 4 | 3.0–4.0 | 272.133, 660.387, 911.497, 953.580, 1164.582, 1435.706, 1487.628 |
| 5 | 4.0–5.0 | 205.095, 573.309, 585.367, 642.388, 1085.694, 1227.626, 2741.410, 2913.678, 2927.693, 2941.668, 2981.607, 3025.066 |
| 6 | 5.0–5.6 | 497.400, 771.408, 939.662, 1148.716, 1423.836, 2218.047 |
| 7 | 5.6–6.1 | 378.163, 487.319, 728.497, 1418.844, 1439.702, 1548.844, 5297.517, 6211.754 |
| 8 | 6.1–6.3 | 403.251, 555.356, 656.346, 1074.574, 1127.483, 1265.684, 1447.679, 1719.983 |
| 9 | 6.3–6.8 | 753.455, 969.590, 1105.569, 1534.865, 1587.776, 2068.808, 2229.234, 3251.858 |
| 10 | 6.8–7.1 | 419.237, 638.392, 1056.622, 1247.703, 1702.955 |
| 11 | 7.1–7.7 | 1060.438, 1378.768, 2208.189, 3015.057, 3251.857 |
| 12 | 7.7–8.3 | 918.474, 1499.748, 3152.777, 4089.223 |
| 13 | 8.3–8.6 | 900.542, 1128.687, 1182.607, 1250.760, 1266.756, 1500.731, 2244.169, 4716.118 |
| 14 | 8.6–9.0 | 813.492, 1072.654, 1258.713, 2913.497 |
| 15 | 9.0–10.0 | 1365.787, 1452.818, 1902.932, 2765.478 |
| 16 | 10.0–11.0 | 918.557, 995.474, 1281.875, 1415.896, 1840.016, 1893.933 |
| 17 | 11.0–11.8 | 1274.625, 1593.932, 1645.945, 1689.987, 3640.506 |
| 18 | 11.8–12.3 | 1761.009, 1991.029, 2043.940, 2091.104, 2291.182 |
| 19 | 12.3–12.7 | 1324.985, 1689.951 |
| 20 | 12.7–13.8 | 1317.740, 1518.891, 1856.998, 1909.904 |