Table 5.
Peptide sequences analyzed from MS/MS spectra.
| Fr | RT | Intens. × 103 |
MSMS m/z |
Charge | (M + H)+ | Sequence |
|---|---|---|---|---|---|---|
| 1 | 1.23 | 70 | 251.499 | 3+ | 752.482 | SKLHRL-NH2 |
| 2 | 1.95 | 85 | 253.116 | + | 253.116 | SF |
| 3 | 2.09 | 91 | 459.905 | 3+ | 1377.700 | RGPRTYSHGHPL |
| 2.27 | 1500 | 318.204 | 3+ | 952.596 | SLSKLHRL-NH2 | |
| 2.53 | 8 | 304.481 | 3+ | 911.428 | TYSHGHPL | |
| 2.78 | 35 | 366.648 | 2+ | 732.288 | HNAEFD | |
| 4 | 3.06 | 8 | 318.532 | 3+ | 953.580 | SLSKLHRL |
| 3.34 | 72 | 330.697 | 2+ | 660.387 | LSEALK | |
| 3.55 | 330 | 456.253 | 2+ | 911.497 | PRLPRLT | |
| 3.66 | 750 | 479.240 | 3+ | 1435.706 | RDPRTYSHGHPL | |
| 3.80 | 1500 | 388.865 | 3+ | 1164.582 | PRTYSHGHPL | |
| 5 | 4.06 | 42 | 293.187 | 2+ | 585.367 | LSPLR |
| 4.56 | 350 | 287.159 | 2+ | 573.309 | RPPGF | |
| 4.99 | 60 | 321.698 | 2+ | 642.388 | GLSPLR | |
| 6 | 5.18 | 85 | 383.577 | 3+ | 1148.716 | VPSLKSLHRL-NH2 |
| 5.37 | 90 | 386.208 | 2+ | 771.408 | RPPGFTP | |
| 5.60 | 29 | 313.893 | 3+ | 939.662 | LVKQKVLL-NH2 | |
| 7 | 5.79 | 80 | 378.163 | + | 378.163 | DFP |
| 6.00 | 90 | 364.751 | 2+ | 728.495 | LKSLLVG-NH2 | |
| 8 | 6.07 | 8 | 403.251 | + | 403.251 | LTGL |
| 6.26 | 600 | 358.863 | 3+ | 1074.574 | RPPGFTPFR (Thr6-BK) | |
| 9 | 6.41 | 11 | 377.231 | 2+ | 753.455 | RLPGLTP |
| 6.45 | 62,000 | 512.294 | 3+ | 1534.865 | PRLRRLTGLSPLR | |
| 6.74 | 860 | 323.869 | 3+ | 969.590 | PATLPAPFR | |
| 10 | 6.84 | 210 | 416.572 | 3+ | 1247.703 | RLVKPVPFYE |
| 6.94 | 1200 | 352.879 | 3+ | 1056.622 | RLPGLTPFR | |
| 7.02 | 12,000 | 568.324 | 3+ | 1702.955 | PRLRRLTGLSPLRAP | |
| 11 | 7.63 | 85 | 530.723 | 2+ | 1060.438 | HNAEFDAAW |
| 7.67 | 390 | 689.887 | 2+ | 1378.768 | PRLRRLTGLSPL | |
| 12 | 7.80 | 52 | 459.741 | 2+ | 918.474 | RPPGFTPF |
| 13 | 8.57 | 2200 | 564.848 | 2+ | 1128.687 | LSEALKSLLVG-NH2 |
| 14 | 8.72 | 470 | 536.829 | 2+ | 1072.650 | LSEALKSLLV |
| 8.73 | 160 | 407.249 | 2+ | 813.490 | PATLPAPF | |
| 8.84 | 460 | 629.861 | 2+ | 1258.713 | LSEALKSLLVGE | |
| 15 | 9.07 | 45 | 455.934 | 3+ | 1365.787 | DALPRLLPAPFR |
| 9.17 | 31 | 484.945 | 3+ | 1452.818 | DALPRLLPGTPFR | |
| 9.70 | 135 | 634.982 | 3+ | 1902.932 | DTFGPLYDKLHQYLGH-NH2 | |
| 16 | 10.69 | 16 | 427.964 | 3+ | 1281.875 | FLLPLLKGLLVG-NH2 |
| 10.81 | 28 | 472.637 | 3+ | 1415.896 | GLLTDLRKFLLK-NH2 | |
| 10.95 | 16 | 459.783 | 2+ | 918.557 | GLVYLLQL | |
| 17 | 11.72 | 9 | 549.320 | 3+ | 1645.945 | DDGLLTDLRKFLLK-NH2 |
| 18 | 11.92 | 30 | 697.706 | 3+ | 2091.104 | HPDDDDDFLLPLLKGLLVG-NH2 |
| 12.01 | 1600 | 664.348 | 3+ | 1991.029 | DDDDDGLLTDLRKFLLK-NH2 | |
| 20 | 13.11 | 1050 | 619.669 | 3+ | 1856.992 | DDDDDFLLPLLKGLLVG-NH2 |