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Reagents and conditions: (a)311 KOAc, AcOH, chlorobenzene, reflux, 2 days; (b) LiAlH4, THF, 0 °C to rt; (c) 156.2, KOAc, AcOH, chlorobenzene, reflux, 2 days; (d) (1) LiAlH4, THF, 0 °C to rt, (2) 156.2, KOAc, AcOH, chlorobenzene, reflux, 2 days.
