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. 2021 Dec 1;122(1):565–788. doi: 10.1021/acs.chemrev.1c00449

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© 2021 The Authors. Published by American Chemical Society

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Scheme 167 — Reagents and conditions: (a)³³⁶ (1) cis-[Ru(bpy)₂Cl₂]·2H₂O, AgClO₄, EtOH, reflux, 1 h, (2) 167.1, reflux, 10 h; (b) (1) cis-Os(bpy)₂Cl₂, EtOH, water, reflux, 40 h, (2) NaClO₄, rt; (c)³³⁸ (1) cis-[Ru(bpy)₂Cl₂]·2H₂O, ethylene glycol, reflux, overnight, (2) NaClO₄, water, rt; (d) (1) cis-Os(bpy)₂Cl₂, ethylene glycol, reflux, overnight, (2) NaClO₄, water, rt.