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. 2021 Dec 1;122(1):565–788. doi: 10.1021/acs.chemrev.1c00449

Scheme 174. Synthesis of Oxygen- and Nitrogen-Doped Twistacenes.

Scheme 174

Reagents and conditions: (a)348 1-naphthol, PPh3, Cs2CO3, Pd(OAc)2, DMF, 140 °C, 24 h; (b)349 catechol, NaH, NMP, 205 °C, 12 h; (c) 2-aminophenol, NaH, NMP, 205 °C, 12 h; (d)350 K2CO3, DMF, 110 °C.