Scheme 331. Synthesis of Singly and Doubly Naphthalene-Fused Porphyrins and Anthracene-Bridged Porphyrin Dimers.
Reagents and conditions: (a)616 (1) 2-mesitylmagnesium bromide, dry THF, rt, (2) BF3·OEt2, dry DCM, (3) DDQ, DCM; (b) t-BuOK, THF.
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