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. 2021 Dec 1;122(1):565–788. doi: 10.1021/acs.chemrev.1c00449

Scheme 86. Synthesis of Twisted N-Doped Nanographenes.

Scheme 86

Reagents and conditions: (a)168o-xylene, 80 °C, 30 min, then reflux, 12 h; (b) DDQ, TfOH, DCM (high dilution), 0 °C to rt, 4 h.