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a Reaction conditions: graphite felt (GF) anode and Ag cathode, 1 (0.1 mmol), NH3 (balloon, ca. 1 atm), Mg(ClO4)2 (0.1 mmol), MeOH/DCM = 4 mL/1 mL, or 3 mL/2 mL, 3.5–4.5 V cell potential, rt, 3–4 h. [a] isolated yields are reported for all cases. [b] reaction conditions: GF anode and Ag cathode, 1aq (0.05 mmol), Mg(ClO4)2 (0.1 mmol), MeOH/toluene = 3 mL/2 mL, 5.5 V cell potential, rt, 3 h. b Substrates did not react.
