Figure 1.
Comparison of signal-to-noise (S/N) ratios of 2D 1H-77Se CPMG-HSQMBC spectra obtained on [77Se]DGal and SeDGal samples of 2 mM each. (A) 1H (F2) projection of 2D 1H-77Se correlation spectrum of [77Se]DGal recorded in 13 min, resulting in an S/N = 192.6; (B) representative 2D 1H-77Se correlation spectrum of [77Se]DGal; and (C) 1H (F2) projection of 2D 1H-77Se correlation spectrum of nonenriched SeDGal recorded in 3.5 h, resulting in an S/N = 58.6.