Table 2.
Analytes | Nominal concentration (ng/mL) | Intrabatch (n = 5) | Interbatch (n = 15) | ||||
---|---|---|---|---|---|---|---|
Measured concentration (ng/mL) | Precision (%) | Accuracy (%) | Measured concentration (ng/mL) | Precision (%) | Accuracy (%) | ||
Trans-resveratrol | 2.24 | 2.30 ± 0.25 | 10.91 | 103.23 | 2.31 ± 0.20 | 8.81 | 103.71 |
5.59 | 5.93 ± 0.56 | 9.45 | 106 | 5.52 ± 0.50 | 9.11 | 98.65 | |
22.35 | 25.24 ± 0.47 | 1.87 | 112.6 | 23.69 ± 2.13 | 9.00 | 105.69 | |
111.75 | 108 ± 4.52 | 4.18 | 96.28 | 107.34 ± 9.02 | 8.40 | 95.79 | |
| |||||||
R3G | 1.00 | 1.07 ± 0.15 | 14.00 | 106.9 | 1.03 ± 0.13 | 12.22 | 103.44 |
5.00 | 5.25 ± 0.30 | 6.00 | 104.9 | 5.33 ± 0.32 | 6.07 | 106.46 | |
20.00 | 18.1 ± 0.91 | 5.00 | 90.48 | 18.31 ± 1.25 | 6.86 | 91.57 | |
100.00 | 90.7 ± 4.67 | 5.00 | 90.7 | 96.21 ± 7.74 | 8.04 | 96.21 | |
| |||||||
R3S | 1.00 | 1.02 ± 0.08 | 8.11 | 101.50 | 0.96 ± 0.09 | 9.38 | 96.05 |
5.00 | 5.19 ± 0.22 | 4.29 | 103.87 | 5.34 ± 0.37 | 6.97 | 106.83 | |
20.00 | 18.04 ± 0.61 | 3.00 | 90.30 | 18.67 ± 1.65 | 8.84 | 93.33 | |
100.00 | 103.07 ± 9.13 | 8.86 | 103.07 | 100.73 ± 10.96 | 10.88 | 100.73 |
Data of measured concentration represented as mean ± SD. R3G, trans-resveratrol-3-o-β-glucuronide; R3S, trans-resveratrol-3-sulfate salt.