| Crystal data |
| Chemical formula |
[Nd2(C5H6O4)(SO4)2(H2O)6] |
|
M
r
|
718.79 |
| Crystal system, space group |
Monoclinic, P21/c
|
| Temperature (K) |
293 |
|
a, b, c (Å) |
15.5461 (1), 12.6621 (1), 8.8883 (1) |
| β (°) |
95.287 (1) |
|
V (Å3) |
1742.19 (3) |
|
Z
|
4 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
6.23 |
| Crystal size (mm) |
0.2 × 0.2 × 0.2 |
| |
| Data collection |
| Diffractometer |
SuperNova, Single source at offset/far, HyPix3000 |
| Absorption correction |
Multi-scan (CrysAlis PRO; Agilent, 2014 ▸) |
|
T
min, T
max
|
0.448, 1.000 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
38711, 3830, 3482 |
|
R
int
|
0.067 |
| (sin θ/λ)max (Å−1) |
0.648 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.022, 0.045, 1.08 |
| No. of reflections |
3830 |
| No. of parameters |
268 |
| No. of restraints |
9 |
| H-atom treatment |
H atoms treated by a mixture of independent and constrained refinement |
| Δρmax, Δρmin (e Å−3) |
0.62, −0.88 |
