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. 2022 Jan 7;78(Pt 2):111–113. doi: 10.1107/S2056989021013554

Table 2. Experimental details.

Crystal data
Chemical formula Cs2SnSi6O15
M r 793.05
Crystal system, space group Monoclinic, I2/c
Temperature (K) 296
a, b, c (Å) 26.3434 (10), 7.4805 (3), 22.9137 (7)
β (°) 107.4020 (7)
V3) 4308.7 (3)
Z 12
Radiation type Mo Kα
μ (mm−1) 7.36
Crystal size (mm) 0.12 × 0.03 × 0.01
 
Data collection
Diffractometer Bruker APEXII CCD
Absorption correction Multi-scan (SADABS; Krause et al., 2015).
T min, T max 0.539, 0.747
No. of measured, independent and observed [I > 2σ(I)] reflections 51032, 8282, 5013
R int 0.077
(sin θ/λ)max−1) 0.772
 
Refinement
R[F 2 > 2σ(F 2)], wR(F 2), S 0.037, 0.082, 1.00
No. of reflections 8282
No. of parameters 331
Δρmax, Δρmin (e Å−3) 1.84, −1.48

Computer programs: APEX3 and SAINT (Bruker, 2018), SHELXT (Sheldrick, 2015a ), SHELXL2018/3 (Sheldrick, 2015b ), ATOMS (Dowty, 2006) and publCIF (Westrip, 2010).