TABLE 6.
Reaction parameters | Production of TMP (g/L) | Conversion rate (%) |
---|---|---|
Molar concentration ratio | ||
2:5 | 33.72 ± 1.43 | 50.72 ± 2.15 |
2.5:5 | 36.04 ± 0.74 | 54.20 ± 1.11 |
3:5 | 33.79 ± 0.78 | 50.81 ± 1.17 |
3.5:5 | 33.46 ± 0.14 | 50.32 ± 0.22 |
4:5 | 29.99 ± 1.01 | 45.10 ± 1.52 |
Time (h) | ||
1 | 33.19 ± 0.07 | 49.91 ± 0.10 |
2 | 36.04 ± 0.74 | 54.20 ± 1.11 |
3 | 36.67 ± 0.56 | 55.15 ± 0.84 |
4 | 32.58 ± 0.41 | 48.99 ± 0.62 |
5 | 30.77 ± 0.18 | 46.27 ± 0.27 |
Temperature (°C) | ||
90 | 36.67 ± 0.56 | 55.15 ± 0.84 |
120 | 37.46 ± 1.25 | 56.33 ± 1.88 |
150 | 40.58 ± 2.02 | 61.03 ± 3.04 |
180 | 45.64 ± 1.61 | 68.64 ± 2.42 |
210 | 42.06 ± 0.34 | 63.25 ± 0.51 |
Rotation speed (rpm) | ||
200 | 45.64 ± 1.61 | 68.64 ± 2.42 |
400 | 46.48 ± 0.38 | 69.90 ± 0.57 |
600 | 44.17 ± 0.77 | 66.43 ± 1.16 |
800 | 42.77 ± 0.48 | 64.32 ± 0.73 |
1,200 | 40.23 ± 0.34 | 60.50 ± 0.51 |
SD, standard deviation, n = 3.